2-(4-甲氧基苯基)-1,3-二氧戊环合成路线 (共 29 条)
反应条件
dihydrogen peroxide; vanadium pentoxide in water T=5°C; 3 h;
参考文献
Gopinath, Rangam; Paital, Alok Ranjan; Patel, Bhisma K
Tetrahedron Letters, 2002 , vol. 43, # 29 p. 5123 - 5126
反应条件
CoCl2.6H2O; zinc in tetrahydrofuran T=20°C; 4 h;
参考文献
Sarma, Kuladip; Goswami, Amrit
Letters in Organic Chemistry, 2009 , vol. 6, # 7 p. 568 - 572
反应条件
lithium aluminium tetrahydride; zirconium tetrachloride in diethyl ether T=30°C; Reduction; 12 h;
参考文献
Shaozu, Wu; Tianhui, Ren; Ning, Chen; Yulan, Zhang
Organic Preparations and Procedures International, 1991 , vol. 23, # 4 p. 427 - 431
参考文献
Chemical Communications, , # 3 p. 327 - 328
反应条件
lithium aluminium tetrahydride; zirconium tetrachloride in diethyl ether 7 h; Heating; Yield given. Yields of byproduct given;
参考文献
Shaozu, Wu; Yulan, Zhang; Tianhui, Ren
Gazzetta Chimica Italiana, 1991 , vol. 121, # 9 p. 445 - 447
反应条件
lithium aluminium tetrahydride; (η5-C5H5)titanium trichloride in diethyl ether 12 h; Heating; Title compound not separated from byproducts;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 100, # 5 p. 421 - 424
反应条件
hydrogenchloride; hydroxylamine hydrochloride in ethanol 2 h; Heating;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 41, # 11 p. 2042 - 2043
反应条件
pyridinium hydrobromide perbromide; orthoformic acid triethyl ester in 1,2-dichloro-ethane T=50°C; 2 h;
参考文献
Tetrahedron Letters, , vol. 46, # 12 p. 1989 - 1992
反应条件
tetra-n-butylammonium tribromide in tetrahydrofuran
T=20°C; 0.08 h;
参考文献
Naik, Sarala; Gopinath, Rangam; Goswami, Mousumi; Patel, Bhisma K.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 11 p. 1670 - 1677
反应条件
acetyl chloride in methanol
0.5 h; RefluxGreen chemistry; TemperatureTime; chemoselective reaction;
参考文献
Yu, Hai-Feng
Synthetic Communications, 2013 , vol. 43, # 9 p. 1280 - 1286