(2E)-1-(4-溴苯基)-3-苯基-2-丙烯-1-酮合成路线 （共 11 条）
反应条件
1: 58 percent / CH2Cl2 / 40 - 42 °C 2: 60 percent / KOH / ethanol / Heating View Scheme
参考文献
Prakash, Om; Kumar, Rajesh; Sharma, Deepak; Pannu, Kamaljeet; Kamal, Raj
Synlett, 2007 , # 14 p. 2189 - 2192
反应条件
1: Reaktion ueber mehrere Stufen 2: durch Verseifung 3: glacial acetic acid; hydrogen bromide 5: alkali View Scheme
参考文献
Kohler, Hill, Bigelow
Journal of the American Chemical Society, 1917 , vol. 39, p. 2414
反应条件
sodium in dichloromethane T=20°C; 3 h;
参考文献
Konduru, Naveen Kumar; Dey, Sunita; Sajid, Mohammad; Owais, Mohammad; Ahmed, Naseem
European Journal of Medicinal Chemistry, 2013 , vol. 59, p. 23 - 30
参考文献
Weygand
Justus Liebigs Annalen der Chemie, 1927 , vol. 459, p. 112
Justus Liebigs Annalen der Chemie, 1929 , vol. 472, p. 178
反应条件
boron trifluoride diethyl etherate; urea T=140°C; Microwave irradiation;
参考文献
Borthakur, Moyurima; Dutta, Mandakini; Gogoi, Shyamalee; Boruah, Romesh C.
Synlett, 2008 , # 20 p. 3125 - 3128
反应条件
(Ph)2SiH2; zinc(II) chloride; tetrakis(triphenylphosphine) palladium(0) in chloroform 3 h; Ambient temperature;
参考文献
Keinan, Ehud; Greenspoon, Noam
Journal of the American Chemical Society, 1986 , vol. 108, # 23 p. 7314 - 7325
反应条件
benzyl-N,N-dimethylamine in methanol
7 h; Heating;
参考文献
Orlov, V. D.; Kolos, N. N.; Yaremenko, F. G.; Lavrushin, V. F.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1980 , vol. 16, # 5 p. 547 - 550
Khimiya Geterotsiklicheskikh Soedinenii, 1980 , # 5 p. 697 - 700
反应条件
1: 70 percent perchloric acid / 1) 2 h, 90 deg C, 2) ethanol, 1 h, reflux
2: 58 percent / 25 percent aq. NH3 / ethanol / Heating
View Scheme
参考文献
Fischer, Gerhard W.; Zimmermann, Thomas; Weissenfels, Manfred
Journal fuer Praktische Chemie (Leipzig), 1983 , vol. 325, # 5 p. 729 - 741
反应条件
1: 70 percent perchloric acid / 1) 2 h, 90 deg C, 2) ethanol, 1 h, reflux
2: 79 percent / Et3N / Heating
View Scheme
参考文献
Fischer, Gerhard W.; Zimmermann, Thomas; Weissenfels, Manfred
Journal fuer Praktische Chemie (Leipzig), 1983 , vol. 325, # 5 p. 729 - 741
反应条件
morpholine in ethanol
Ambient temperature;
参考文献
Shestopalov, A. M.; Promonenkov, V. K.; Sharanin, Yu. A.; Rodinovskaya, L. A.; Sharanin, S. Yu.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 7 p. 1382 - 1401
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 7 p. 1517 - 1538
