2,3,5,6-四氯吡啶合成路线 （共 54 条）
参考文献
Iddon, Brian; Mack, Arthur G.; Suschitzky, Hans; Taylor, Jack A.; Wakefield, Basil J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1370 - 1380
反应条件
sodium hydride in N,N-dimethyl-formamide
1.) r.t., 30 min, 2.) r.t., 24 h;
参考文献
Xu, Xiaoyong; Qian, Xuhong; Li, Zhong; Song, Gonghua
Journal of Fluorine Chemistry, 1998 , vol. 88, # 1 p. 9 - 13
反应条件
1: 95 percent / dimethylformamide / 3 h / 120 °C
2: 55 percent / 3 h / 64 °C
View Scheme
参考文献
Schmidt, Andreas; Mordhorst, Thorsten; Nieger, Martin
Tetrahedron, 2006 , vol. 62, # 8 p. 1667 - 1674
反应条件
caesium carbonate in DMF (N,N-dimethyl-formamide)
T=20 - 70°C; 4 - 6 h;
参考文献
COUNCIL OF SCIENTIFIC AND INDUSTRIAL RESEARCH
Patent: WO2004/87667 A1, 2004 ;
Location in patent: Page 17 ;
