2,3,5,6-四氯吡啶合成路线 (共 54 条)
反应条件
ammonium chloride; methanephosphonic acid dimethyl ester; zinc in water 0.5 h; Yield given;
参考文献
Journal of Heterocyclic Chemistry, , vol. 17, p. 493 - 496
参考文献
Luxembourg Industries (Pamol) Ltd.
Patent: US5618942 A1, 1997 ;
反应条件
hydrogenchloride; zinc in (2S)-N-methyl-1-phenylpropan-2-amine hydrate; water; methanephosphonic acid dimethyl ester
反应条件
copper; benzoyl chloride in N,N-dimethyl-formamide T=150°C; 0.5 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1682 - 1687
反应条件
1: With copper(l) chloride in nitrobenzene T=95 - 135°C; P=760.051 Torr; 20 h; Inert atmosphere; 2: in nitrobenzene T=135 - 140°C; P=760.051 Torr; 2 h;
参考文献
Organic Process Research and Development, , vol. 7, # 3 p. 329 - 333
反应条件
copper in N,N-dimethyl-formamide T=150°C;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1682 - 1687
反应条件
para-xylene; copper in N,N-dimethyl-formamide T=150°C; 1 h; Further byproducts given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1682 - 1687
反应条件
in diethyl ether 19 h; Irradiation;
参考文献
Bratt, Jack; Iddon, Brian; Mack, Arthur G.; Suschitzky, Hans; Taylor, Jack A.; Wakefield, Basil J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 648 - 656
反应条件
Copper(I)chloride in acetonitrile