1,1'-(2,2'-联苯二基)二乙酮合成路线 (共 20 条)
反应条件
N-phenyl-2-pyridinecarboxamide; copper in acetonitrile
T=20°C; Ullmann Condensation; 20 h; Inert atmosphere; Time;
参考文献
Damkaci, Fehmi; Altay, Esra; Waldron, Matthew; Knopp, Michael A.; Snow, David; Massaro, Nicholas
Tetrahedron Letters, 2014 , vol. 55, # 3 p. 690 - 693
反应条件
1: With zinc in tetrahydrofuran
Heating;
2: With (3,5-dinitrophenyl)(4-methylpiperazin-1-yl)methanone; copper(I) bromide dimethylsulfide complex in N,N-dimethyl acetamide
T=22°C; 1 h;
参考文献
Su, Xianbin; Fox, David J.; Blackwell, David T.; Tanaka, Kiyotaka; Spring, David R.
Chemical Communications, 2006 , # 37 p. 3883 - 3885
反应条件
potassium carbonate; palladium on activated charcoal in ethylene glycol dimethyl ether
Suzuki homocoupling reaction; 0.333333 h; microwave irradiation;
参考文献
Cravotto, Giancarlo; Beggiato, Marina; Penoni, Andrea; Palmisano, Giovanni; Tollari, Stefano; Leveque, Jean-Marc; Bonrath, Werner
Tetrahedron Letters, 2005 , vol. 46, # 13 p. 2267 - 2271
反应条件
zinc; NiCl2((PPh3)P)2 in N,N-dimethyl-formamide
T=60°C; Ullmann-pinacol coupling; 24 h;
参考文献
Lin, Shuang-Zheng; Chen, Qing-An; You, Tian-Pa
Synlett, 2007 , # 13 p. 2101 - 2105
反应条件
NiCl2((PPh3)P)2; zinc in N,N-dimethyl-formamide
T=60°C; Ullmann-pinacol coupling; 24 h;
参考文献
Lin, Shuang-zheng; You, Tian-pa
Tetrahedron, 2008 , vol. 64, # 42 p. 9906 - 9910
反应条件
[2,2']bipyridinyl; potassium iodide; NiBr2bipy in various solvent(s)
Ambient temperatureelectrochemical coupling;
参考文献
Meyer, Gilbert; Rollin, Yolande; Perichon, Jacques
Journal of Organometallic Chemistry, 1987 , vol. 333, p. 263 - 268
反应条件
[2,2']bipyridinyl; NiBr2bipy in various solvent(s)
T=20°C; electrochemical reaction, magnesium anode, gold gauze cathode, -1,2 V; Yield given. Yields of byproduct given;
参考文献
Rollin, Yolande; Troupel, Michel; Tuck, Dennis G.; Perichon, Jacques
Journal of Organometallic Chemistry, 1986 , vol. 303, p. 131 - 138
反应条件
bis(p-methoxyphenyl)tellurone
参考文献
Engman, Lars; Cava, Michael P.
Journal of the Chemical Society, Chemical Communications, 1982 , # 3 p. 164 - 165
反应条件
chromium(VI) oxide; water; acetic acid
T=70°C;
参考文献
Hall et al.
Journal of the Chemical Society, 1956 , p. 3475,3480
反应条件
NaH-t-AmONa-Ni(OAc)2-bpy-KI
1.) benzene/THF, 63 deg C, 2.5 h; Yield given. Multistep reaction;
参考文献
Lourak, Mouhsine; Vanderesse, Regis; Fort, Yves; Caubere, Paul
Journal of Organic Chemistry, 1989 , vol. 54, # 20 p. 4840 - 4844