反应条件
1: 70 percent / triethylamine, 4-dimethylaminopyridine (DMAP) / CH2Cl2 / 2 h / Ambient temperature 3: 97 percent / triethylamine, 4-dimethylaminopyridine (DMAP) / CH2Cl2 / 2 h / Ambient temperature 4: 1.) sodium hydride / 1.) DMF, 80 deg C, 2.5 h, 2.) DMF, 80 deg C, 24 h 5: 71 percent / phenol, 33percent HBr in acetic acid / 60 h / 80 °C View Scheme
参考文献
Acta Chemica Scandinavica, , vol. 45, # 6 p. 621 - 626
