aluminium T=60 - 70°C; und auf 110-120grad;

in diethyl ether; toluene i-PrMgBr in diethyl ether is added dropwise to well-stirred and refluxing toluene, suspn. is cooled to room temp., anhydrous AlCl3 is added, stirred at room temp. overnight; ppt. is centrifuged, vac. distn.;

暂无反应条件数据

phosphorus trichoride

in isopropyl alcohol stirring (1 h, room temp.), H2O addn. (room temp.), ageing period (1 h),filtering, washing (5x, hot water), drying (18 h, 383 K), moistening, d rying (24 h, 383 K), calcination (air, 2 h, 573 K), heating (2 h, 773 K); composition determination;

in Petroleum ether

in not given