3,5-二碘-4-甲氧基苄肼合成路线 (共 2 条)
反应条件
hydrazine hydrate in methanol 2 h; Inert atmosphereReflux;
参考文献
Grimster, Neil P.; Connelly, Stephen; Baranczak, Aleksandra; Dong, Jiajia; Krasnova, Larissa B.; Sharpless, K. Barry; Powers, Evan T.; Wilson, Ian A.; Kelly, Jeffery W.
Journal of the American Chemical Society, 2013 , vol. 135, # 15 p. 5656 - 5668
反应条件
1.1: potassium carbonate / N,N-dimethyl-formamide / 20 °C / |Inert atmosphere 1.2: 20 °C / |Inert atmosphere 2.1: hydrazine hydrate / methanol / 2 h / |Inert atmosphere; |Reflux View Scheme
参考文献
Grimster, Neil P.; Connelly, Stephen; Baranczak, Aleksandra; Dong, Jiajia; Krasnova, Larissa B.; Sharpless, K. Barry; Powers, Evan T.; Wilson, Ian A.; Kelly, Jeffery W.
Journal of the American Chemical Society, 2013 , vol. 135, # 15 p. 5656 - 5668