1,2-双(二甲基瞵)乙烷合成路线 （共 25 条）
参考文献
Pure and Applied Chemistry, , vol. 61, p. 1701 - 1706
反应条件
in tetrahydrofuran T=50°C; 2 h; Thermodynamic data;
参考文献
Canadian Journal of Chemistry, , vol. 79, # 5-6 p. 626 - 631
反应条件
in benzene dropwise addn. of phosphine to Rh-compound in benzene (N2, Schlenk tube technique), stirring for 1h at room temp., filtn., washing with ether, drying in vac., dissolving in methanol, addn. of NH4PF6, stirring for 10 min; addn. of ether, filtn., washing with ether, recrystn. (acetone/ether);
参考文献
Werner, Helmut; Hofmann, Lothar; Paul, Wilfried; Schubert, Ulrich
Organometallics, 1988 , vol. 7, p. 1106 - 1111
反应条件
in tetrahydrofuran T=50°C; 2 h; Thermodynamic data;
参考文献
Smith D.C.; Cadoret; Jafarpour; Stevens; Nolan
Canadian Journal of Chemistry, 2001 , vol. 79, # 5-6 p. 626 - 631
反应条件
in petroleum ether
Irradiation (UV/VIS); under N2, educts dissolved in petroleum ether, photolyzed for 22 h; evapd. in vac., dried in vac. at room temp., sublimed (80°C, 1E-2 Torr), recrystd. from petroleum ether; elem. anal.;
参考文献
Dudeney, Nicholas; Green, Jennifer C.; Grebenik, Peter; Kirchner, Olaf N.
Journal of Organometallic Chemistry, 1983 , vol. 252, # 2 p. 221 - 230
