4-氯-1-(2,4-二氯苯氧基)-2-硝基苯合成路线 （共 7 条）
反应条件
1: 2,4-dichloro-phenol With potassium hydroxide in water T=110°C; 2: 1-nitro-2,5-dichloro-benzene in water T=150°C;
参考文献
DORF KETAL CHEMICALS (I) PRIVATE LIMITED
Patent: WO2009/90669 A2, 2009 ;
Location in patent: Page/Page column 20 ;
反应条件
phosphorus pentachloride; chlorine T=170°C;
参考文献
Matsui; Obokata
Yuki Gosei Kagaku Kyokaishi, 1955 , vol. 13, p. 590,594
Chem.Abstr., 1957 , p. 2217
反应条件
nitric acid; acetic acid
参考文献
Groves; Turner; Sharp
Journal of the Chemical Society, 1929 , p. 521
参考文献
Matsui; Obokata
Yuki Gosei Kagaku Kyokaishi, 1955 , vol. 13, p. 590,594
Chem.Abstr., 1957 , p. 2217
参考文献
Journal of the Chemical Society, , p. 521
反应条件
1: SnCl2; aqueous methanol.HCl
2: aqueous hydrochloric acid; sodium nitrite / Erwaermen des Reaktionsgemisches mit Kupfer(I)-chlorid und wss. Salzsaeure
View Scheme
参考文献
Matsui; Obokata
Yuki Gosei Kagaku Kyokaishi, 1955 , vol. 13, p. 590,594
Chem.Abstr., 1957 , p. 2217
反应条件
1: H2 / Raney-Ni / dioxane
2: 115 h / Heating
View Scheme
参考文献
Fuhrer,H. et al.
Journal of Heterocyclic Chemistry, 1979 , vol. 16, p. 1121 - 1134
