3-甲氧基吡嗪 1-氧化物合成路线 (共 16 条)
反应条件
dihydrogen peroxide in water; acetic acid T=65 - 68°C; 17 h;
参考文献
SYNGENTA PARTICIPATIONS AG
Patent: WO2003/87067 A1, 2003 ;
Location in patent: Page/Page column 38-39 ;
反应条件
N,N-diethylaniline; trichlorophosphate 2 h; Heating / reflux;
参考文献
WO2003/87067 A1, ;
Page/Page column 39 ;
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene; trichlorophosphate 2 h; Heating; Yield given. Yields of byproduct given;
参考文献
Sato, Nobuhiro; Fujii, Megumi
Journal of Heterocyclic Chemistry, 1994 , vol. 31, # 5 p. 1177 - 1180
反应条件
trichlorophosphate 2 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Sato, Nobuhiro
Journal of Chemical Research, Miniprint, 1984 , # 10 p. 2860 - 2875
反应条件
trichlorophosphate 2 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Sato, Nobuhiro
Journal of Chemical Research, Miniprint, 1984 , # 10 p. 2860 - 2875
反应条件
N,N-diethylaniline; trichlorophosphate 2 h; Heating / reflux;
参考文献
SYNGENTA PARTICIPATIONS AG
Patent: WO2003/87067 A1, 2003 ;
Location in patent: Page/Page column 39 ;
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene; trichlorophosphate 2 h; Heating; Yield given. Yields of byproduct given;
参考文献
Sato, Nobuhiro; Fujii, Megumi
Journal of Heterocyclic Chemistry, 1994 , vol. 31, # 5 p. 1177 - 1180
反应条件
trichlorophosphate 2 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Sato, Nobuhiro
Journal of Chemical Research, Miniprint, 1984 , # 10 p. 2860 - 2875
反应条件
trichlorophosphate 2 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Sato, Nobuhiro
Journal of Chemical Research, Miniprint, 1984 , # 10 p. 2860 - 2875
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene; trichlorophosphate 2 h; Heating; Yield given. Yields of byproduct given;
参考文献
Sato, Nobuhiro; Fujii, Megumi
Journal of Heterocyclic Chemistry, 1994 , vol. 31, # 5 p. 1177 - 1180