in tetrachloromethane byproducts: benzene, iso-C3H7OH, C3H6O; sealed evacuated H-shaped ampuls; react. of Ph3BiCl2 and Li-compd. in CCl4 at 20°C (168 h); transcondensation of lig. products with cooling (liq. N2) into a limb of the ampul, hydrolyzation of solid residue by aq. THF, codensation of alcohol into a trap (liq. N2), treatement of solid residue (hexane, water); detn. of lig. products by GLC anal.;
参考文献
Journal of General Chemistry USSR (English Translation), , vol. 54, p. 87 - 89
Zhurnal Obshchei Khimii, , vol. 54, p. 100 - 103
