2-甲基-3-苯基喹唑啉-4(3H)-酮合成路线 （共 32 条）
反应条件
1: ethanol / 5 h / 0 - 20 °C
2: potassium iodide / ethanol; water / 6 h / 20 °C
3: piperidine / 20 - 50 °C
View Scheme
参考文献
Kumar, R. Arun; Maheswari, C. Uma; Ghantasala, Satheesh; Jyothi; Reddy, K. Rajender
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 2-3 p. 401 - 410
反应条件
1.1: benzene / 5 h / Reflux; Dean Stark apparatus
1.2: 20 °C
2.1: platinum(IV) oxide; hydrogen / ethanol / 20 °C
3.1: ethanol / 5 h / 0 - 20 °C
4.1: potassium iodide / ethanol; water / 6 h / 20 °C
5.1: piperidine / 20 - 50 °C
View Scheme
参考文献
Kumar, R. Arun; Maheswari, C. Uma; Ghantasala, Satheesh; Jyothi; Reddy, K. Rajender
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 2-3 p. 401 - 410
反应条件
1.1: benzene / 5 h / Reflux; Dean Stark apparatus
1.2: 20 °C
2.1: platinum(IV) oxide; hydrogen / ethanol / 20 °C
3.1: ethanol / 5 h / 0 - 20 °C
4.1: potassium iodide / ethanol; water / 6 h / 20 °C
5.1: piperidine / 20 - 50 °C
View Scheme
参考文献
Kumar, R. Arun; Maheswari, C. Uma; Ghantasala, Satheesh; Jyothi; Reddy, K. Rajender
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 2-3 p. 401 - 410
参考文献
Meyer; Wagner
Journal of Organic Chemistry, 1943 , vol. 8, p. 239,249
参考文献
Meyer; Wagner
Journal of Organic Chemistry, 1943 , vol. 8, p. 239,249
反应条件
1: dichloromethane / 5 h / 0 - 20 °C
2: tetrahydrofuran / 1 h / -78 °C
View Scheme
参考文献
Nakano, Hayato; Kutsumura, Noriki; Saito, Takao
Synthesis (Germany), 2012 , vol. 44, # 20 p. 3179 - 3184
反应条件
1: dichloromethane / 4 h / 0 - 20 °C / |Inert atmosphere
2: dichloromethane / 5 h / 0 - 20 °C
3: tetrahydrofuran / 1 h / -78 °C
View Scheme
参考文献
Nakano, Hayato; Kutsumura, Noriki; Saito, Takao
Synthesis (Germany), 2012 , vol. 44, # 20 p. 3179 - 3184
反应条件
trichlorophosphate; benzene
参考文献
Kossur; Weil
Roczniki Chemii, 1938 , vol. 18, p. 161,166
Chem. Zentralbl., 1939 , vol. 110, # II p. 1492
反应条件
anschliessendes Erhitzen mit Phosphor(III)-chlorid in Toluol;
参考文献
Grimmel; Guenther; Morgan
Journal of the American Chemical Society, 1946 , vol. 68, p. 539
参考文献
Grimmel; Guenther; Morgan
Journal of the American Chemical Society, 1946 , vol. 68, p. 539
