2-甲基-1H-苯并(去)异喹啉-1,3(2H)-二酮合成路线 (共 19 条)
反应条件
2,6-dichloro-benzonitrile; potassium tert-butylate T=170°C;
参考文献
Sakamoto; Pac
Journal of Organic Chemistry, 2001 , vol. 66, # 1 p. 94 - 98
反应条件
bei Siedetemperatur;unter zutritt von Luft;
参考文献
Bradley; Pexton
Journal of the Chemical Society, 1954 , p. 4436,4437
反应条件
in ethanol; water
T=20°C; 72 h; Inert atmosphere;
参考文献
Nicholson, Brian K.; Crosby, Paul M.; Maunsell, Kieran R.; Wyllie, Megan J.
Journal of Organometallic Chemistry, 2012 , vol. 716, p. 49 - 54
反应条件
in acetonitrile
Irradiation;
参考文献
Yoon, Ung Chan; Kim, Dong Uk; Lee, Chan Woo; Choi, Young Sun; Lee, Yean-Jang; Ammon, Herman L.; Mariano, Patrick S.
Journal of the American Chemical Society, 1995 , vol. 117, # 10 p. 2698 - 2710
反应条件
palladium diacetate; triethylamine; triphenylphosphine in N,N-dimethyl-formamide
T=50°C; P=45004.5 Torr; 72 h; Autoclave; chemoselective reaction;
参考文献
Takacs, Attila; Petz, Andrea; Kollar, Laszlo
Tetrahedron, 2010 , vol. 66, # 25 p. 4479 - 4483
反应条件
tert.-butylhydroperoxide; copper(l) chloride in dichloromethane; water
T=50°C; 24 h; Sealed tube;
参考文献
Yan, Xiaoyu; Fang, Kun; Liu, Hailan; Xi, Chanjuan
Chemical Communications, 2013 , vol. 49, # 90 p. 10650 - 10652
反应条件
in acetonitrile
2.5 h; Irradiation;
参考文献
Yoon, Ung Chan; Kim, Dong Uk; Lee, Chan Woo; Choi, Young Sun; Lee, Yean-Jang; Ammon, Herman L.; Mariano, Patrick S.
Journal of the American Chemical Society, 1995 , vol. 117, # 10 p. 2698 - 2710
反应条件
in acetonitrile
2.5 h; Irradiation;
参考文献
Yoon, Ung Chan; Kim, Dong Uk; Lee, Chan Woo; Choi, Young Sun; Lee, Yean-Jang; Ammon, Herman L.; Mariano, Patrick S.
Journal of the American Chemical Society, 1995 , vol. 117, # 10 p. 2698 - 2710
反应条件
acrylonitrile in acetonitrile
Irradiation;
参考文献
Takahashi, Yasutake; Miyashi, Tsutomu; Yoon, Ung Chan; Oh, Sun Wha; Mancheno, Maria; Su, Zhuoyi; Falvey, Daniel F.; Mariano, Patrick S.
Journal of the American Chemical Society, 1999 , vol. 121, # 16 p. 3926 - 3932
反应条件
1: With [2,2']bipyridinyl; nickel dichloride; zinc in N,N-dimethyl-formamide
T=70°C; 6 h;
2: With dihydrogen peroxide in N,N-dimethyl-formamide
T=30 - 40°C; 0.5 h;
参考文献
Adonin; Ryabinin; Starichenko
Russian Journal of Organic Chemistry, 2000 , vol. 36, # 6 p. 861 - 865