反应条件
in water; acetone addn. of the Fe-salt to a stirred soln. of 2 equiv. KCN in 20percent aq. acetone at 0°C under N2; storing for 1 h; pouring into ethyl acetate;; washing with brine, cold 5percent hydrochloric acid, aq. sodium bicarbonate and water; drying the organic layer over Na2SO4; evaporation under reduced pressure; radial chromy. with hexane/ethyl acetate (5:1) as eluent;;
参考文献
Ong, Chi Wi; Chien, Chen Jeng
Organometallics, 1993 , vol. 12, p. 241 - 243
