(4-甲基苄基)三苯基溴化膦合成路线 （共 21 条）
反应条件
in toluene 18 h; Heating;
参考文献
Traylor T. G.; Stewart, Kevin J.
Journal of the American Chemical Society, 1986 , vol. 108, # 22 p. 6977 - 6985
反应条件
in diethyl ether Ambient temperature;
参考文献
Pearson, Morwenna S. M.; Carbery, David R.
Journal of Organic Chemistry, 2009 , vol. 74, # 15 p. 5320 - 5325
反应条件
1: PBr3 / diethyl ether / -40 °C 2: benzene / 20 °C View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 48, # 2 p. 556 - 568
反应条件
1: NBS, benzoylperoxide / 3 h / Heating 2: CHCl3 / 2 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 42, # 15 p. 4161 - 4168
反应条件
1: sodium tetrahydroborate / methanol / 1 h / 20 °C 2: phosphorus tribromide / benzene / 20 °C 3: toluene / 120 °C View Scheme
参考文献
Journal of Steroid Biochemistry and Molecular Biology, , vol. 137, p. 332 - 344
反应条件
1: (4-methyl-benzyl)-triphenyl-phosphonium bromide With sodium hydride in ethylene glycol dimethyl ether T=0°C; Wittig reaction; 1 h; Inert atmosphere; 2: 4-chlorobenzaldehyde in ethylene glycol dimethyl ether T=60°C; Wittig reaction; 9 h; Inert atmosphere;
参考文献
Shimojuh, Naoya; Imura, Yumi; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron, 2011 , vol. 67, # 5 p. 951 - 957
反应条件
1.1: n-butyllithium / tetrahydrofuran / 12 h / -78 - 20 °C / Inert atmosphere 1.2: 12 h / Inert atmosphere 2.1: iodine; methyloxirane / cyclohexane / Irradiation; Inert atmosphere 3.1: 1100 °C / 0.08 Torr / Pyrolysis View Scheme
参考文献
Amsharov, Konstantin Yu.; Kabdulov, Mikhail A.; Jansen, Martin
European Journal of Organic Chemistry, 2009 , # 36 p. 6328 - 6335
反应条件
potassium carbonate in 1,4-dioxane
参考文献
Journal of the American Chemical Society, , vol. 108, # 22 p. 6977 - 6985
反应条件
sodium methylate in methanol Wittig reaction;
参考文献
Sancho-Garcia, Juan Carlos; Bredas, Jean-Luc; Beljonne, David; Cornil, Jerome; Martinez-Alvarez, Roberto; Hanack, Michael; Poulsen, Lars; Gierschner, Johannes; Mack, Hans-Georg; Egelhaaf, Hans-Joachim; Oelkrug, Dieter
Journal of Physical Chemistry B, 2005 , vol. 109, # 11 p. 4872 - 4880
反应条件
1: (4-methyl-benzyl)-triphenyl-phosphonium bromide With n-butyllithium in tetrahydrofuran; hexane T=-15°C; 0.5 h; 2: β-naphthaldehyde in tetrahydrofuran; hexane T=-15 - 20°C; Wittig reaction;
参考文献
Pearson, Morwenna S. M.; Carbery, David R.
Journal of Organic Chemistry, 2009 , vol. 74, # 15 p. 5320 - 5325
