1,5-戊二醇二甲烷磺酸酯合成路线 （共 6 条）
反应条件
triethylamine in dichloromethane T=0 - 20°C; 2 h;
参考文献
Fer, Mickael J.; Olatunji, Samir; Bouhss, Ahmed; Calvet-Vitale, Sandrine; Gravier-Pelletier, Christine
Journal of Organic Chemistry, 2013 , vol. 78, # 20 p. 10088 - 10105
反应条件
in pyridine; dichloromethane T=25°C;
参考文献
Ehrsson; Hassan
Journal of Pharmaceutical Sciences, 1983 , vol. 72, # 10 p. 1203 - 1205
反应条件
sodium iodide in acetone T=70°C; 0.333333 h;
参考文献
Ehrsson; Hassan
Journal of Pharmaceutical Sciences, 1983 , vol. 72, # 10 p. 1203 - 1205
反应条件
1: acetone 2: ethanol 3: hydrazine hydrate; ethanol / Erwaermen des Reaktionsprodukts mit wss. Salzsaeure 4: pyridine 5: sodium sulfide nonahydrate; ethanol View Scheme
参考文献
May and Baker Ltd.
Patent: US2830008 , 1956 ;
反应条件
1: acetone
2: ethanol
3: platinum; ethanol / Hydrogenation
View Scheme
参考文献
May and Baker Ltd.
Patent: US2830008 , 1956 ;
反应条件
potassium carbonate in acetonitrile
8 h; Reflux;
参考文献
Pei, Dong; Zhang, Yu; Wei, Siyu; Wang, Meng; Sun, Jian
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 4 p. 619 - 623
