4-溴-2,6-二甲基苯酚合成路线 (共 34 条)
反应条件
N,N,N-trimethyl-1-phenylmethanaminium tribromide in methanol; dichloromethane
参考文献
Kakinami; Suenaga; Yamaguchi; Okamoto; Kajigaeshi
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 10 p. 3373 - 3375
反应条件
1: With 2,3-benzodioxin-1,4-dione Heating; 2: With water; sodium hydrogencarbonate in methanol T=40°C; Overall yield = 73 percent;
参考文献
Nature, , vol. 499, # 7457 p. 192 - 196
反应条件
1-benzyl-1-aza-4-azoniabicyclolt;2.2.2gt;octane bromide; calcium carbonate in methanol T=20°C; 0.25 h;
参考文献
Hajipour, Abdol R.; Pourmousavi, Seied A.; Ruoho, Arnold E.
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 3 p. 796 - 800
反应条件
diethyl 2,2-dibromomalonate T=100°C; Bromination; aromatization; 48 h;
参考文献
Coumbarides; Dingjan; Eames; Weerasooriya
Journal of Chemical Research - Part S, 2000 , # 7 p. 328 - 329
反应条件
potassium bromide in water T=25°C; enolization, pH dependencs, catalytic effect of various acids; Rate constant;
参考文献
Journal of the American Chemical Society, , vol. 107, # 2 p. 455 - 459
反应条件
in diethyl ether T=37°C; 24 h; Further byproducts given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2617 - 2625
反应条件
in diethyl ether T=37°C; 22 h; Further byproducts given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2617 - 2625
反应条件
1: Br2, aq. HCl 2: (i) aq. NaNO2, H2SO4, (ii) aq. HBr, CuBr, Cu View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 44, p. 2248 - 2253
反应条件
in diethyl ether 18 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 51, # 2 p. 174 - 179
反应条件
(i) aq. NaNO2, H2SO4, (ii) aq. HBr, CuBr, Cu; Multistep reaction;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 44, p. 2248 - 2253