3,4-(亚甲二氧)肉桂酸合成路线 （共 62 条）
反应条件
aluminum oxide; lithium chloride Doebner condensation; 0.1 h; microwave irradiation;
参考文献
Mogilaiah; Reddy, G. Randheer
Synthetic Communications, 2004 , vol. 34, # 2 p. 205 - 210
反应条件
1: With water; sodium hydroxide in tetrahydrofuran 2: With hydrogenchloride in water pH=< 3;
参考文献
Pedersen, Mikael E.; Metzler, Bjorn; Stafford, Gary I.; Van Staden, Johannes; Jaeger, Anna K.; Rasmussen, Hasse B.
Molecules, 2009 , vol. 14, # 9 p. 3833 - 3843
反应条件
pyridine; acetic acid T=130°C; Knoevenagel-Doebner reaction; 0.133333 h; microwave irradiation;
参考文献
Tetrahedron, , vol. 63, # 4 p. 960 - 965
反应条件
potassium acetate 6 h; Heating;
参考文献
Terada; Motomiya; Yoshioka; Narita; Yasui; Takase
Chemical and Pharmaceutical Bulletin, 1987 , vol. 35, # 6 p. 2437 - 2442
反应条件
1: 1.) LDA, 2.) CBr4 / 1) THF, -78 deg C (45 min), 0 deg C (3 1/4 h), RT (1 h); 2) THF, -78 deg C, 2 h 2: 92 percent / KI / acetone / 24 h / Heating 3: NaH / 0 °C 4: 1.) LDA View Scheme
参考文献
Synthetic Communications, , vol. 18, # 7 p. 699 - 710
反应条件
1: 304 mg / conc. H2SO4 / 1 h / Heating 2: K2CO3, Cu0 / dimethylformamide / 1 h / Heating 3: 15 mg / KOH / ethanol; H2O / Heating View Scheme
参考文献
Phytochemistry (Elsevier), , vol. 23, # 5 p. 1029 - 1036
反应条件
1: K2CO3, Cu0 / dimethylformamide / 1 h / Heating 2: 15 mg / KOH / ethanol; H2O / Heating View Scheme
参考文献
Phytochemistry (Elsevier), , vol. 23, # 5 p. 1029 - 1036
参考文献
Chemische Berichte, , vol. 86, p. 190,196
反应条件
1: 92 percent / KI / acetone / 24 h / Heating 2: NaH / 0 °C 3: 1.) LDA View Scheme
参考文献
Synthetic Communications, , vol. 18, # 7 p. 699 - 710
反应条件
1: pyridine; piperidine 2: ethanolic KOH-solution View Scheme
参考文献
Chemische Berichte, , vol. 86, p. 190,196
