戊烷-1,5-二(溴化镁)合成路线 （共 50 条）
反应条件
1: 65 percent / tetrahydrofuran
2: 65 percent / Jones reagent / acetone / 1 h / 0 °C
View Scheme
参考文献
Canonne, Persephone; Foscolos, Georges B.; Belanger, Denis
Journal of Organic Chemistry, 1980 , vol. 45, # 10 p. 1828 - 1835
反应条件
hydrogenchloride
1.) THF, overnight, 2.) 40 deg C, 1h; Yield given. Multistep reaction;
参考文献
Canonne, Persephone; Belanger, Denis
Journal of the Chemical Society, Chemical Communications, 1980 , # 3 p. 125 - 126
反应条件
1: With cis-2,10-dimethyl-lt;1,2,3gt;benzothiadiphosphololt;2,3-bgt;lt;1,2,3gt;benzothiadiphosphole in tetrahydrofuran
2: in tetrahydrofuran
T=20°C; Acid hydrolysis;
参考文献
Baccolini, Graziano; Boga, Carla; Galeotti, Matteo
Angewandte Chemie - International Edition, 2004 , vol. 43, # 23 p. 3058 - 3060
参考文献
Gmelin Handbook: Ge: SVol., 128, page 554 - 556
反应条件
1: 67 percent / tetrahydrofuran
2: 94 percent / Jones reagent / acetone / 1 h / 0 °C
View Scheme
参考文献
Canonne, Persephone; Foscolos, Georges B.; Belanger, Denis
Journal of Organic Chemistry, 1980 , vol. 45, # 10 p. 1828 - 1835
反应条件
hydrogenchloride
1.) THF, overnight, 2.) 40 deg C, 1h; Yield given. Multistep reaction;
参考文献
Canonne, Persephone; Belanger, Denis
Journal of the Chemical Society, Chemical Communications, 1980 , # 3 p. 125 - 126
反应条件
1: diethyl ether
2: benzene
View Scheme
参考文献
Gmelin Handbook: Sn: Org.Verb.3, 1.1.6.1.3, page 105 - 108
反应条件
in diethyl ether
react. at 0°C, boiling for 0.5h;;
参考文献
Zappi, E. V.
Anales Asoc. Quim. Arg., 1920 , vol. 8, p. 55 - 66
Full Text Show Details
Gmelin Handbook: Sn: Org.Verb.3, 1.1.6.1.3, page 105 - 108
参考文献
Canonne, Persephone; Foscolos, Georges B.; Belanger, Denis
Journal of Organic Chemistry, 1980 , vol. 45, # 10 p. 1828 - 1835
反应条件
1: diethyl ether
2: alcoholic KOH-solution
View Scheme
参考文献
Lespieau
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1924 , vol. 178, p. 1566
Bulletin de la Societe Chimique de France, 1925 , vol. <4>37, p. 423
