甲基-6-叠氮-6-脱氧-alpha-D-吡喃葡萄糖苷合成路线 （共 5 条）
参考文献
Griffith, Byron R.; Krepel, Candace; Fu, Xun; Blanchard, Sophie; Ahmed, Aqeel; Edmiston, Charles E.; Thorson, Jon S.
Journal of the American Chemical Society, 2007 , vol. 129, # 26 p. 8150 - 8155
反应条件
hydrogen in methanol
18 h;
参考文献
Burland, Peter A.; Osborn, Helen M.I.; Turkson, Andrea
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 18 p. 5679 - 5692
反应条件
With methanol; sodium methylate T=20°C; 0.0333333 h; sonication;
参考文献
Deng, Shenglou; Gangadharmath, Umesh; Chang, Cheng-Wei Tom Journal of Organic Chemistry, 2006 , vol. 71, # 14 p. 5179 - 5185
反应条件
Multi-step reaction with 5 steps 1: 94 percent / pyridine / 3 h / Ambient temperature2: 2.2 g / 1M methanolic ammonia / 6 h / Ambient temperature3: 68 percent / sodium azide, ammonium chloride / dimethylformamide / 1.2 h / Heating4: 1.) 1.4 M methanolic hydrochloric acid / 1.) reflux, 1.5 h; 2.) pyridine, roomtemp., overnight5: 82 percent / barium hydroxide octahydrate / methanol / 0.17 h / Ambient temperature
参考文献
Matsuda; Tsuchiya; Torii; Umezawa Bulletin of the Chemical Society of Japan, 1986 , vol. 59, # 5 p. 1397 - 1401
反应条件
Multi-step reaction with 4 steps 1: 2.2 g / 1M methanolic ammonia / 6 h / Ambient temperature2: 68 percent / sodium azide, ammonium chloride / dimethylformamide / 1.2 h / Heating3: 1.) 1.4 M methanolic hydrochloric acid / 1.) reflux, 1.5 h; 2.) pyridine, roomtemp., overnight4: 82 percent / barium hydroxide octahydrate / methanol / 0.17 h / Ambient temperature
参考文献
Matsuda; Tsuchiya; Torii; Umezawa Bulletin of the Chemical Society of Japan, 1986 , vol. 59, # 5 p. 1397 - 1401
