1,3-二氯-2,4,6-三氟苯合成路线 （共 16 条）
反应条件
copper; zinc in water; N,N-dimethyl-formamide T=70°C; 10 h;
参考文献
Russian Journal of Organic Chemistry, , vol. 36, # 10 p. 1488 - 1499
反应条件
1: With n-butyllithium T=-78°C; 2: With water T=-78 - 20°C;
参考文献
Casares, Juan A.; Espinet, Pablo; Martin-Alvarez, Jose M.; Martinez-Ilarduya, Jesus M.; Salas, Gorka
European Journal of Inorganic Chemistry, 2005 , # 19 p. 3825 - 3831
反应条件
1: iron; aqueous NH4Cl 3: sulfuryl chloride; disulfur dichloride; aluminium chloride View Scheme
参考文献
Journal of the American Chemical Society, , vol. 73, p. 153
Journal of the American Chemical Society, , vol. 81, p. 94,98
反应条件
1: sulfuric acid; aqueous phosphoric acid; nitrosylsulfuric acid / anschliessendes Behandeln mit Natriumhypophosphit-Loesung und Kupfer(I)-oxid 2: iron; aqueous NH4Cl 4: sulfuryl chloride; disulfur dichloride; aluminium chloride View Scheme
参考文献
Journal of the American Chemical Society, , vol. 73, p. 153
Journal of the American Chemical Society, , vol. 81, p. 94,98
反应条件
2: sulfuryl chloride; disulfur dichloride; aluminium chloride View Scheme
参考文献
Journal of the American Chemical Society, , vol. 73, p. 153
Journal of the American Chemical Society, , vol. 81, p. 94,98
反应条件
1: H2SO4; HNO3 2: sulfuric acid; aqueous phosphoric acid; nitrosylsulfuric acid / anschliessendes Behandeln mit Natriumhypophosphit-Loesung und Kupfer(I)-oxid 3: iron; aqueous NH4Cl 5: sulfuryl chloride; disulfur dichloride; aluminium chloride View Scheme
参考文献
Journal of the American Chemical Society, , vol. 73, p. 153
Journal of the American Chemical Society, , vol. 81, p. 94,98
反应条件
disulfur dichloride; aluminium trichloride; sulfuryl dichloride
参考文献
Journal of the American Chemical Society, , vol. 73, p. 153
Journal of the American Chemical Society, , vol. 81, p. 94,98
反应条件
disulfur dichloride; aluminium trichloride; sulfuryl dichloride
参考文献
Journal of the American Chemical Society, , vol. 73, p. 153
Journal of the American Chemical Society, , vol. 81, p. 94,98
反应条件
zinc copper in water; N,N-dimethyl-formamide T=70°C; 10 h; other polyfluoroarenes and polyfluorinated olefins; other temperature and time;
参考文献
Russian Journal of Organic Chemistry, , vol. 30, # 8 p. 1336 - 1340
Zhurnal Organicheskoi Khimii, , vol. 30, # 8 p. 1271 - 1275
反应条件
p-benozquinone; bis(.mu.-bromo)bis(5-(pentafluorophenyl)-1-3-.eta.3-cyclohexadienyl)dipalladium(II) in chloroform-d1 T=50°C; 4 h; Product distribution; Further Variations:Reagentstime;
参考文献
Chemistry - A European Journal, , vol. 7, # 11 p. 2481 - 2489
