N-(P-甲基苯亚甲基)苯胺合成路线 (共 44 条)
反应条件
1: triethylamine / dichloromethane / 0 - 20 °C
2: [RuIII(2,4-pentanedionato)3]; 1,1,1-tris (diphenylphosphinomethyl)ethane; methanesulfonic acid; hydrogen / tetrahydrofuran / 16 h / 200 °C / 7500.75 Torr / |Autoclave; |Inert atmosphere
View Scheme
参考文献
Coetzee, Jacorien; Dodds, Deborah L.; Klankermayer, Juergen; Brosinski, Sandra; Leitner, Walter; Slawin, Alexandra M. Z.; Cole-Hamilton, David J.
Chemistry - A European Journal, 2013 , vol. 19, # 33 p. 11039 - 11050
参考文献
Song, Qing-Wen; Yu, Bing; Liu, An-Hua; He, Ying; Yang, Zhen-Zhen; Diao, Zhen-Feng; Song, Qing-Chuan; Li, Xue-Dong; He, Liang-Nian
RSC Advances, 2013 , vol. 3, # 41 p. 19009 - 19014
反应条件
in acetonitrile
T=24.84°C; Thermodynamic data;
参考文献
Zhu, Xiao-Qing; Liu, Qiao-Yun; Chen, Qiang; Mei, Lian-Rui
Journal of Organic Chemistry, 2010 , vol. 75, # 3 p. 789 - 808
反应条件
NiCuFeO(x) in anhydrous xylene
4 h; Inert atmosphereReflux;
参考文献
Cui, Xinjiang; Dai, Xingchao; Deng, Youquan; Shi, Feng
Chemistry - A European Journal, 2013 , vol. 19, # 11 p. 3665 - 3675
反应条件
diborane in methanol
0.5 h; Ambient temperature;
参考文献
Nose, Atsuko; Kudo, Tadahiro
Chemical and Pharmaceutical Bulletin, 1986 , vol. 34, # 11 p. 4817 - 4820
反应条件
bis(η3-allyl-μ-chloropalladium(II)) in benzene
T=65°C; 7 h;
参考文献
Iovel; Golomba; Fleisher; Popelis; Grinberga; Lukevics
Chemistry of Heterocyclic Compounds, 2004 , vol. 40, # 6 p. 701 - 714
反应条件
hydrochloric ether; carbon dioxide in N,N-dimethyl-formamide
参考文献
Hess, U.; Thiele, R.
Journal fuer Praktische Chemie (Leipzig), 1982 , vol. 324, # 3 p. 385 - 399
反应条件
mercury dichloride; zinc in ethanol; chloroform
4.5 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Smith, James G.; Boettger, Thomas J.
Synthetic Communications, 1981 , vol. 11, # 1 p. 61 - 64
反应条件
in acetic acid
4 h; Heating;
参考文献
Rajendar Reddy, K.; Mogilaiah, K.; Sreenivasulu, B.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 1194 - 1196
反应条件
3-hydroxy-2-phenyl-quinazoline-(3H)-4-one
Irradiation;
参考文献
Sahadeva Reddy; Pratap Reddy; Reddy
Synthetic Communications, 2001 , vol. 31, # 22 p. 3447 - 3451