反式-2-苯基-1-环已醇合成路线 （共 72 条）
参考文献
Price; Karabinos
Journal of the American Chemical Society, 1940 , vol. 62, p. 1159
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Eliel et al.
Journal of Organic Chemistry, 1957 , vol. 22, p. 1533,1538
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Schaeffer; Collins
Journal of the American Chemical Society, 1956 , vol. 78, p. 124,130
参考文献
Price; Karabinos
Journal of the American Chemical Society, 1940 , vol. 62, p. 1159
反应条件
(1S,3R,4S,5R,7R)-N-hydroxy-4-benzyl-1-isopropyl-2-azaadamantane; sodium hydrogencarbonate in dichloromethane T=-40°C; 3 h; Resolution of racemateInert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Hamada, Shohei; Wada, Yoshiyuki; Sasamori, Takahiro; Tokitoh, Norihiro; Furura, Takumi; Kawabata, Takeo
Tetrahedron Letters, 2014 , vol. 55, # 11 p. 1943 - 1945
反应条件
N-chloro-succinimide; (S)-(-)-2,2'-bis(diphenylphosphino)-1,1'-binaphthyl in tetrahydrofuran T=20°C; 0.166667 h;
参考文献
Sekar; Nishiyama
Journal of the American Chemical Society, 2001 , vol. 123, # 15 p. 3603 - 3604
反应条件
(S,S)(4-JandaJel-CH2-O(CH2)3O)-2(BnN(Me)CH2)N(Me)pyrrolidine; 4 A molecular sieve; triethylamine in dichloromethane T=-78°C; 11 h;
参考文献
Clapham; Cho; Janda
Journal of Organic Chemistry, 2001 , vol. 66, # 3 p. 868 - 873
参考文献
Carpenter, Bryon E.; Hunt, Ian R.; Keay, Brian A.
Tetrahedron Asymmetry, 1996 , vol. 7, # 11 p. 3107 - 3108
反应条件
(S)-HBTM; N-ethyl-N,N-diisopropylamine in chloroform-d1 T=20°C; 3 h; optical yield given as percent ee;
参考文献
Harada, Shingo; Kuwano, Satoru; Yamaoka, Yousuke; Yamada, Ken-Ichi; Takasu, Kiyosei
Angewandte Chemie - International Edition, 2013 , vol. 52, # 39 p. 10227 - 10230
Angew. Chem., 2013 , vol. 125, # 39 p. 10417 - 10420,4
反应条件
(-)-sparteine in acetonitrile electrolysis: 'H' type divided cell separated by membrane Nafion 117, NaClO4 as supporting electrolyte, TEMPO-modified grafite felt electrode, charge passed 1.17 F mol-1, electrolysis potential 0.60 V (vs. Ag/AgCl);
参考文献
Chemical Communications, , # 24 p. 2745 - 2746
反应条件
4-(N,N-dimethlyamino)pyridine in dichloromethane T=20°C; 24 h;
参考文献
Matsugi, Masato; Hagimoto, Yuri; Nojima, Masatomo; Kita, Yasuyuki
Organic Process Research and Development, 2003 , vol. 7, # 4 p. 583 - 584
反应条件
Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Ding, Jie; Welton, Thomas; Armstrong, Daniel W.
Analytical Chemistry, 2004 , vol. 76, # 22 p. 6819 - 6822
