1,6-萘啶-2(1H)-酮合成路线 （共 14 条）
反应条件
hydrogenchloride in water 4 h; Heating;
参考文献
Turner, James A.
Journal of Organic Chemistry, 1990 , vol. 55, # 15 p. 4744 - 4750
反应条件
sodium ethanolate in ethanol 2 h; Heating;
参考文献
Sakamoto, Takao; Kondo, Yoshinori; Yamanaka, Hiroshi
Chemical & Pharmaceutical Bulletin, 1985 , vol. 33, # 11 p. 4764 - 4768
反应条件
1: 65 percent / tris(o-tolyl)phosphine, Et3N / Pd(OAc)2 / acetonitrile / 48 h / 120 °C 2: 67 percent / EtONa / ethanol / 2 h / Heating View Scheme
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 33, # 11 p. 4764 - 4768
反应条件
selenium(IV) oxide in acetic acid 24 h; Heating;
参考文献
Singh, Baldev; Lesher, George Y.
Journal of Heterocyclic Chemistry, 1990 , vol. 27, # 7 p. 2085 - 2091
反应条件
sulfuric acid 50 h; Heating;
参考文献
Wozniak, M.; Plas, H. C. van der; Tomula, M.; Veldhuizen, A. van
Recueil: Journal of the Royal Netherlands Chemical Society, 1983 , vol. 102, # 7-8 p. 359 - 363
反应条件
1: 75 percent / dimethylformamide / 22 h / Ambient temperature 2: 100 percent / ammonium acetate / dimethylformamide / 3 h / 120 - 130 °C 3: 90 percent / 50percent aq. H2SO4 / 18 h / 135 - 140 °C 4: 52 percent / various solvent(s) / 0.67 h / Heating 5: 51 percent / SeO2 / acetic acid / 24 h / Heating View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 27, # 7 p. 2085 - 2091
反应条件
1: 90 percent / 50percent aq. H2SO4 / 18 h / 135 - 140 °C 2: 52 percent / various solvent(s) / 0.67 h / Heating 3: 51 percent / SeO2 / acetic acid / 24 h / Heating View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 27, # 7 p. 2085 - 2091
反应条件
1: 52 percent / various solvent(s) / 0.67 h / Heating 2: 51 percent / SeO2 / acetic acid / 24 h / Heating View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 27, # 7 p. 2085 - 2091
反应条件
1: 100 percent / ammonium acetate / dimethylformamide / 3 h / 120 - 130 °C 2: 90 percent / 50percent aq. H2SO4 / 18 h / 135 - 140 °C 3: 52 percent / various solvent(s) / 0.67 h / Heating 4: 51 percent / SeO2 / acetic acid / 24 h / Heating View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 27, # 7 p. 2085 - 2091
反应条件
1: 1.) KNH2; 2.) KMnO4 / 1.) liquid NH3, 15 min; 2.) liquid NH3, 10 min 2: 80 percent / 80 percent aq. sulphuric acid / 50 h / Heating View Scheme
参考文献
Recueil: Journal of the Royal Netherlands Chemical Society, , vol. 102, # 7-8 p. 359 - 363
