反应条件
1: 1,2-bis-(2-hydroxyethoxy)-ethane With sodium hydride in tetrahydrofuran 0.25 h; Cooling with iceInert atmosphere; 2: 8-Methoxy-1-(methylsulfonyl)oxy-3,6-dioxaoctane in tetrahydrofuran Cooling with iceReflux;
参考文献
Scates, Bradley A.; Lashbrook, Bethany L.; Chastain, Benjamin C.; Tominaga, Kaoru; Elliott, Brandon T.; Theising, Nicholas J.; Baker, Thomas A.; Fitch, Richard W.
Bioorganic and Medicinal Chemistry, 2008 , vol. 16, # 24 p. 10295 - 10300