双(2-二苯基膦乙基)苯基磷合成路线 （共 3 条）
反应条件
2,2'-azo-bisisobutyronitrile
参考文献
Zeitschrift fuer Chemie (Stuttgart, Germany), , vol. 11, p. 188 - 189
反应条件
(i) aq. HBr, AcOH, (ii) /BRN= 3598720/, PE, Et2O; Multistep reaction;
参考文献
Journal of the Chemical Society, , p. 1490 - 1494
反应条件
in tetrahydrofuran Schlenk techniques used; protective gas: N2; detailed description given; mixture of triphos and of W(CO)3PMTA in THF; reflux (3 h);; evapn.; washing (hexane); filtration (through alumina/CH2Cl2); evapn.to dryness; recrystn. (CH2Cl2/hexane/-20°C);;
参考文献
Zanotti, Valerio; Rutar, V.; Angelici, Robert J.
Journal of Organometallic Chemistry, 1991 , vol. 414, # 2 p. 177 - 191
