2-甲氧基-1,4-萘醌合成路线 (共 80 条)
反应条件
MgCl2*6H2O; toluene-4-sulfonic acid in methanol
5 h; Reflux;
参考文献
Francisco, Acacio I.; Vargas, Maria D.; Carneiro, J. Walkimar de M.; Lanznaster, Mauricio; Torres, Jose C.; Camara, Celso A.; Pinto, Angelo C.
Journal of Molecular Structure, 2008 , vol. 891, # 1-3 p. 228 - 232
反应条件
in tetrahydrofuran
0 deg C, 1 h, RT, 1 h, 55 deg C, 0.5 h; Further byproducts given;
参考文献
Matsuo, Koji; Shiraki, Ryuji; Okubo, Masao
Journal of Physical Organic Chemistry, 1994 , vol. 7, # 10 p. 567 - 577
参考文献
Fieser
Journal of the American Chemical Society, 1926 , vol. 48, p. 2927,2929
Journal of the American Chemical Society, 1928 , vol. 50, p. 439,443
参考文献
Silveira, Gleiciani Q.; Ronconi, Celia M.; Vargas, Maria D.; Gil, Rosane A. S. San; Magalhaes, Alvicler
Journal of the Brazilian Chemical Society, 2011 , vol. 22, # 5 p. 961 - 967
反应条件
dihydrogen peroxide; sodium hydrogencarbonate
参考文献
Anderson,H.A.; Thomson,R.H.
Journal of the Chemical Society [Section] C: Organic, 1966 , p. 426 - 428
反应条件
1: 2-methoxy-1,4-naphthalenequinone With sodium dithionite in 1,4-dioxane; water
1 h;
2: dimethyl sulfate With potassium hydroxide
T=20°C; 3 h;
参考文献
Kimachi, Tetsutaro; Torii, Eri; Kobayashi, Yusuke; Doe, Misae; Ju-Ichi, Motoharu
Chemical and Pharmaceutical Bulletin, 2011 , vol. 59, # 6 p. 753 - 756
反应条件
MgCl2*6H2O; toluene-4-sulfonic acid in methanol
5 h; RefluxDarkness;
参考文献
Francisco, Acacio I.; Vargas, Maria D.; Carneiro, J. Walkimar de M.; Lanznaster, Mauricio; Torres, Jose C.; Camara, Celso A.; Pinto, Angelo C.
Journal of Molecular Structure, 2008 , vol. 891, # 1-3 p. 228 - 232
反应条件
in tetrahydrofuran
0 deg C, 1 h, RT, 1 h, 55 deg C, 0.5 h;
参考文献
Matsuo, Koji; Shiraki, Ryuji; Okubo, Masao
Journal of Physical Organic Chemistry, 1994 , vol. 7, # 10 p. 567 - 577
参考文献
Porter; Skelton; Bowman; Folkers
Journal of medicinal chemistry, 1972 , vol. 15, # 5 p. 504 - 506
反应条件
sodium azide; sulfuric acid
T=25°C; 20 h;
参考文献
Guzikowski, Anthony P.; Cai, Sui Xiong; Espitia, Stephen A.; Hawkinson, Jon E.; Huettner, James E.; Nogales, Daniel F.; Tran, Minhtam; Woodward, Richard M.; Weber, Eckard; Keana, John F. W.
Journal of Medicinal Chemistry, 1996 , vol. 39, # 23 p. 4643 - 4653