2-苯基萘-1,4-二酮合成路线 (共 49 条)
反应条件
Iron (III) nitrate nonahydrate; dipotassium peroxodisulfate in water
T=70°C; 24 h; Schlenk technique; Time;
参考文献
Deb, Arghya; Manna, Srimanta; Maji, Arun; Dutta, Uttam; Maiti, Debabrata
European Journal of Organic Chemistry, 2013 , # 24 p. 5251 - 5256
反应条件
potassium carbonate; (1-benzothiazol-2-yl-ethanone oxime)dichloropalladium(II) in toluene
T=150°C; Suzuki-Miyaura cross-coupling; 0.133333 h; microwave irradiation;
参考文献
Khodade, Vinayak S.; Dharmaraja, Allimuthu T.; Chakrapani, Harinath
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 11 p. 3766 - 3769
反应条件
1: in anhydrous butyl ether
T=130°C; 0.0833333 h; microwave irradiation;
2: With ammonium cerium(IV) nitrate in anhydrous butyl ether
0.333333 h; Further stages.;
参考文献
Hutchinson, Edward J.; Kerr, William J.; Magennis, Euan J.
Chemical Communications, 2002 , # 19 p. 2262 - 2263
反应条件
bis(acetylacetonato) palladium; dimethyl sulfoxide; 2,2,2-trimethylacetic acid
T=140°C; 24 h; Sealed tube;
参考文献
Zhang, Shuai; Song, Feijie; Zhao, Dongbing; You, Jingsong
Chemical Communications, 2013 , vol. 49, # 40 p. 4558 - 4560
反应条件
1: in tetrahydrofuran
T=45°C; Cycloaddition; 16 h;
2: With ammonium cerium(IV) nitrate; water; nitric acid in diethyl ether
Oxidation;
参考文献
Davies; Johnson; Harrity
Journal of Organic Chemistry, 2001 , vol. 66, # 10 p. 3525 - 3532
反应条件
1-methyl-pyrrolidin-2-one; [Pd2(dibenzylideneacetone)3]*dibenzylideneacetone
T=23°C; 16 h;
参考文献
Echavarren, Antonio M.; Frutos, Oscar de; Tamayo, Nuria; Noheda, Pedro; Calle, Paloma
Journal of Organic Chemistry, 1997 , vol. 62, p. 4524 - 4527
反应条件
chromium(VI) oxide in acetic acid
参考文献
Pluim, Henk; Wynberg, Hans
Journal of Organic Chemistry, 1980 , vol. 45, # 12 p. 2498 - 2502
反应条件
tetrakis(triphenylphosphine) palladium(0); copper(I) bromide in 1,4-dioxane
12 h; Heating;
参考文献
Echavarren; Tamayo; Cardenas
Journal of Organic Chemistry, 1994 , vol. 59, # 20 p. 6075 - 6083
反应条件
dipotassium peroxodisulfate; iron(III) sulphate hydrate; oxygen; potassium carbonate in water
T=70°C; 24 h; Green chemistry;
参考文献
Deb, Arghya; Agasti, Soumitra; Saboo, Tapish; Maiti, Debabrata
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 4 p. 705 - 710
反应条件
1: With potassium hydrogensulfate; [RhCl(η2:η2-cycloocta-1,5-diene)]2; cyclooctadiene in butanone
Heating;
2: With sodium periodate; tetrabutylammomium bromide in butanone
T=20°C;
3: With tetrabutylammonium (meta)periodate in butanone
T=20°C;
参考文献
Demchuk, Oleg M.; Pietrusiewicz, K. Michal
Synlett, 2009 , # 7 p. 1149 - 1153