4-[[4-羟基-3-(羟基甲基)苯基]甲基]-2-(羟基甲基)苯酚合成路线 (共 6 条)
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Philip,J.; McLean,J.A.
Journal of Medicinal Chemistry, 1965 , vol. 8, p. 405
反应条件
lithium hydroxide hydrate in water T=20°C; 24 h;
参考文献
Aliouane, Nabila; Helesbeux, Jean-Jacques; Douadi, Tahar; Khan, Mustayeen A.; Bouet, Gilles; Chafaa, Salah; Duval, Olivier
Phosphorus, Sulfur and Silicon and the Related Elements, 2011 , vol. 186, # 2 p. 354 - 364
反应条件
sodium hydroxide in water T=60°C; 1 h; Further byproducts given;
参考文献
Fisher, Thomas H.; Chao, Ping; Upton, Cindy G.; Day, Anthony J.
Magnetic Resonance in Chemistry, 2002 , vol. 40, # 11 p. 747 - 751
反应条件
1: K2CO3 / 165 - 170 °C / 77228.3 Torr 2: LiAlH4; diethyl ether; dioxane View Scheme
参考文献
Seto et al.
Kogyo Kagaku Zasshi, 1955 , vol. 58, p. 382
Chem.Abstr., 1955 , p. 14581
反应条件
1,4-dioxane; lithium aluminium tetrahydride; diethyl ether
参考文献
Carpenter; Hunter
Journal of Applied Chemistry, 1953 , vol. 3, p. 486,493
反应条件
sodium amalgam; ethanol
参考文献
Seto et al.
Kogyo Kagaku Zasshi, 1955 , vol. 58, p. 382
Chem.Abstr., 1955 , p. 14581