1-(3-(苄氧基)-4-甲氧基苯基)乙酮合成路线 （共 12 条）
反应条件
1: 1.) 80 deg C, 1 h; 2.) reflux, 5 h
2: 25.0 g / aq. KOH (50percent) / ethanol / 9 h / Heating
3: 94 percent / HCl / 17 h / 30 °C
4: 97 percent / LiAlH4 / diethyl ether / 2 h / 0 - 20 °C
View Scheme
参考文献
Fujii, Tozo; Ohba, Masashi; Sakaguchi, Jun
Chemical and Pharmaceutical Bulletin, 1987 , vol. 35, # 9 p. 3628 - 3640
反应条件
nitric acid in acetic acid
T=20°C; 3 h;
参考文献
KIRIN BEER KABUSHIKI KAISHA
Patent: EP1447405 A1, 2004 ;
Location in patent: Page 28-29 ;
EP 1447405 A1
