苯并[g][1]苯并二硫杂环戊烷合成路线 （共 42 条）
反应条件
aluminium trichloride; nickel 1.) benzene, 20 deg C, 4 h; 2.) aq. EtOH, 18 h, reflux; Multistep reaction. Title compound not separated from byproducts;
参考文献
Clark, Peter David; McKinnon, David M.
Canadian Journal of Chemistry, 1981 , vol. 59, p. 1297 - 1302
反应条件
aluminium trichloride; nickel 1.) 20 deg C, 4 h; 2.) aq. EtOH, 18 h, reflux; Multistep reaction. Title compound not separated from byproducts;
参考文献
Clark, Peter David; McKinnon, David M.
Canadian Journal of Chemistry, 1981 , vol. 59, p. 1297 - 1302
反应条件
methanesulfonic acid in dichloromethane
T=20°C; 6 h; Inert atmosphereCooling with ice;
参考文献
CANON KABUSHIKI KAISHA; YAMADA, Naoki; KAMATANI, Jun; SAITOH, Akihito
Patent: WO2011/132623 A1, 2011 ;
Location in patent: Page/Page column 29-30 ;
反应条件
chloranil in toluene
48 h; Reflux;
参考文献
Rungtaweevoranit, Bunyarat; Butsuri, Akkarapol; Wongma, Krittaphat; Sadorn, Karoon; Neranon, Kitjanit; Nerungsi, Chakkrapan; Thongpanchang, Tienthong
Tetrahedron Letters, 2012 , vol. 53, # 14 p. 1816 - 1818
反应条件
(THF)W(CO)5 in tetrahydrofuran
T=20°C; Cyclization;
参考文献
Maeyama; Iwasawa
Journal of Organic Chemistry, 1999 , vol. 64, # 4 p. 1344 - 1346
反应条件
in acetonitrile
T=20°C; 16 h; UV-irradiationInert atmospherePyrex filter;
参考文献
Campos-Gomez, Esther; Campos, Pedro J.; Gonzalez, Hector F.; Rodriguez, Miguel A.
Tetrahedron, 2012 , vol. 68, # 22 p. 4292 - 4295
反应条件
dirhodium tetraacetate; lithium tert-butylate in toluene
T=90°C; 1 h; Inert atmosphereMolecular sieve;
参考文献
Xia, Ying; Liu, Zhenxing; Xiao, Qing; Qu, Peiyuan; Ge, Rui; Zhang, Yan; Wang, Jianbo
Angewandte Chemie - International Edition, 2012 , vol. 51, # 23 p. 5714 - 5717
反应条件
barium dihydroxide; copper
T=350°C;
参考文献
Szmuszkovicz; Modest
Journal of the American Chemical Society, 1950 , vol. 72, p. 571,575
反应条件
phosphorus; hydrogen iodide in water
2 h; Heating;
参考文献
Sidorenko, T. N.; Terent'eva, G. A.; Andrienko, O. S.; Savinykh, Yu. V.; Aksenov, V. S.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , p. 156 - 160
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , vol. 19, # 2 p. 192 - 196
反应条件
oxygen in hexane
Cyclization; oxidation; Irradiation;
参考文献
Song, Kai; Wu, Li-Zhu; Yang, Chun-He; Tung, Chen-Ho
Tetrahedron Letters, 2000 , vol. 41, # 12 p. 1951 - 1954
