1-(2-苯并噻唑基硫代)-2-丙酮合成路线 (共 13 条)
反应条件
triethylamine in tetrahydrofuran
参考文献
Yadav; Reddy, P. Venkatram; Chandraiah
Tetrahedron Letters, 2007 , vol. 48, # 1 p. 145 - 148
反应条件
potassium carbonate in tetrahydrofuran 1 h; Heating;
参考文献
Hou, Yankun; Higashiya, Seiichiro; Fuchigami, Toshio
Journal of Organic Chemistry, 1997 , vol. 62, # 26 p. 9173 - 9176
反应条件
hydrogenchloride; tetrafluoroboric acid; sodium iodide; sodium nitrite 1) H2O, 0 deg C, 30 min, 2) acetone, CS2, room temperature, 1-2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Benati, Luisa; Montevecchi, P. Carlo
Journal of Organic Chemistry, 1981 , vol. 46, # 22 p. 4570 - 4573
反应条件
hydrogenchloride; tetrafluoroboric acid; sodium iodide; sodium nitrite 1) H2O, 0 deg C, 30 min, 2) acetone, room temperature, 1-2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Benati, Luisa; Montevecchi, P. Carlo
Journal of Organic Chemistry, 1981 , vol. 46, # 22 p. 4570 - 4573
反应条件
in acetone 3 h; Reagent/catalystSolvent;
参考文献
Al-Omran, Fatima; El-Khair, Adel Abou
Journal of Heterocyclic Chemistry, 2014 , vol. 51, # 1 p. 62 - 70
参考文献
Calo,V. et al.
Gazzetta Chimica Italiana, 1979 , vol. 109, p. 703 - 704
反应条件
sodium iodide multistep reaction, other azidoaniline; Product distribution;
参考文献
Benati, Luisa; Montevecchi, P. Carlo
Journal of Organic Chemistry, 1981 , vol. 46, # 22 p. 4570 - 4573
反应条件
1: 2-(acetonylthio)benzothiazole With carbon disulfide; potassium hydroxide in N,N-dimethyl-formamide T=20°C; 10 h; 2: α-bromoacetophenone in N,N-dimethyl-formamide 6 h; Reflux;
参考文献
Journal of Heterocyclic Chemistry, , vol. 51, # 1 p. 62 - 70
反应条件
1: malononitrile; acetic acid / 1,4-dioxane / 3 h / |Reflux 2: potassium carbonate / acetone / 3 h / |Reflux View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 51, # 1 p. 62 - 70
反应条件
acetic acid; malononitrile in 1,4-dioxane 3 h; Reflux;
参考文献
Al-Omran, Fatima; El-Khair, Adel Abou
Journal of Heterocyclic Chemistry, 2014 , vol. 51, # 1 p. 62 - 70