1: With sulfuric acid; hydroxylamine hydrochloride; acetic acid T=25 - 55°C; 0.5 h; Inert atmosphere; 2: With palladium 10 on activated carbon; hydrogen T=25 - 35°C; P=2585.81 Torr; Inert atmosphere; 3: With hydrogenchloride in ethanol 8 h; Inert atmosphere; Temperature;
参考文献
Roche, Didier; Sans, David; Girgis, Michael J.; Prasad, Kapa; Repic, Oljan; Blacklock, Thomas J.
Organic Process Research and Development, 2001 , vol. 5, # 2 p. 167 - 175
hydrogenchloride; hydrogen; palladium on activated charcoal; palladium dichloride in ethanol P=2585.7 Torr; 8 h;
参考文献
Cannon, Joseph G.; Perez, Julio A.; Pease, Jonathan P; Long, John Paul; Flynn, Jan R.; et al.
Journal of Medicinal Chemistry, 1980 , vol. 23, # 7 p. 745 - 749
