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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
23364-15-0
合成路线
（共 10 条）
56753-76-5
→
反应条件
23364-15-0
反应条件
1: With AlCl3, aluminium chloride in dichloromethane 2 h; Reflux; 2: With water in dichloromethane 0.5 h; Cooling with ice;
参考文献
Dou, Dengfeng; Viwanathan, Prasanth; Li, Yi; He, Guijia; Alliston, Kevin R.; Lushington, Gerald H.; Brown-Clay, Joshua D.; Padmanabhan; Groutas, William C.
Journal of Combinatorial Chemistry, 2010 , vol. 12, # 6 p. 836 - 843
67-56-1
甲醇
+
63586-82-3
→
反应条件
23364-15-0
反应条件
sulfuric acid 8 h; Heating;
参考文献
Janin, Yves L.; Roulland, Emmanuel; Beurdeley-Thomas, Arnaud; Decaudin, Didier; Monneret, Claude; Poupon, Marie-France
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 4 p. 529 - 532
201230-82-2
+
15028-44-1
甲基 3-苯基-DL-丙氨酸酯
+
64-19-7
醋酸
→
反应条件
21156-62-7
N-乙酰基-D-苯基丙氨酸甲酯
+
23364-15-0
反应条件
palladium diacetate; p-benozquinone P=760.051 Torr; 6 h; Reflux;
参考文献
Lopez, Blanca; Rodriguez, Aleix; Santos, David; Albert, Joan; Ariza, Xavier; Garcia, Jordi; Granell, Jaume
Chemical Communications, 2011 , vol. 47, # 3 p. 1054 - 1056
61650-22-4
+
292638-85-8
丙烯酸甲酯
→
反应条件
101301-16-0
+
23364-15-0
反应条件
[{(η5-C5Me5)RhCl}2(μ-Cl)2]; caesium acetate in methanol T=20°C; 16 h;
参考文献
Guimond, Nicolas; Gorelsky, Serge I.; Fagnou, Keith
Journal of the American Chemical Society, 2011 , vol. 133, # 16 p. 6449 - 6457
201230-82-2
+
15028-44-1
甲基 3-苯基-DL-丙氨酸酯
→
反应条件
21156-62-7
N-乙酰基-D-苯基丙氨酸甲酯
+
23364-15-0
反应条件
palladium diacetate; p-benozquinone in acetic acid T=120°C; 6 h; Overall yield = 91 percent;
参考文献
Albert, Joan; Ariza, Xavier; Calvet, Teresa; Font-Bardia, Merce; Garcia, Jordi; Granell, Jaume; Lamela, Andrea; Lopez, Blanca; Martinez, Manuel; Ortega, Laura; Rodriguez, Aleix; Santos, David
Organometallics, 2013 , vol. 32, # 2 p. 649 - 659
495-18-1
苯甲羟肟酸
→
反应条件
101301-16-0
+
23364-15-0
反应条件
1: dichloromethane / 16 h / 20 °C 2: [{(η5-C5Me5)RhCl}2(μ-Cl)2]; caesium acetate / methanol / 16 h / 20 °C View Scheme
参考文献
Guimond, Nicolas; Gorelsky, Serge I.; Fagnou, Keith
Journal of the American Chemical Society, 2011 , vol. 133, # 16 p. 6449 - 6457
23364-15-0
→
反应条件
349552-70-1
1-氯异喹啉-3-羧酸甲酯
反应条件
1: 72 percent / 10percent Pd/C / diphenyl ether / Heating 2: 85 percent / POCl3; K2CO3 / acetonitrile / 1.5 h / Heating View Scheme
参考文献
Janin, Yves L.; Roulland, Emmanuel; Beurdeley-Thomas, Arnaud; Decaudin, Didier; Monneret, Claude; Poupon, Marie-France
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 4 p. 529 - 532
23364-15-0
→
反应条件
89242-09-1
反应条件
1: 72 percent / 10percent Pd/C / diphenyl ether / Heating 2: 82 percent / POBr3; K2CO3 / acetonitrile / 1.5 h / Heating 3: 90 percent / K2PO4 / Pd(PPh3)4 / dimethylformamide / 5 h / 80 °C 4: 95 percent / NaOH / aq. ethanol / 1 h / Heating View Scheme
参考文献
Janin, Yves L.; Roulland, Emmanuel; Beurdeley-Thomas, Arnaud; Decaudin, Didier; Monneret, Claude; Poupon, Marie-France
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 4 p. 529 - 532
23364-15-0
→
反应条件
439614-62-7
反应条件
1: 72 percent / 10percent Pd/C / diphenyl ether / Heating 2: 82 percent / POBr3; K2CO3 / acetonitrile / 1.5 h / Heating View Scheme
参考文献
Janin, Yves L.; Roulland, Emmanuel; Beurdeley-Thomas, Arnaud; Decaudin, Didier; Monneret, Claude; Poupon, Marie-France
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 4 p. 529 - 532
23364-15-0
→
反应条件
63586-82-3
反应条件
1: With lithium hydroxide hydrate in tetrahydrofuran 0.5 h; Cooling with ice; 2: With hydrogenchloride in water pH=2;
参考文献
Dou, Dengfeng; Viwanathan, Prasanth; Li, Yi; He, Guijia; Alliston, Kevin R.; Lushington, Gerald H.; Brown-Clay, Joshua D.; Padmanabhan; Groutas, William C.
Journal of Combinatorial Chemistry, 2010 , vol. 12, # 6 p. 836 - 843
