1-(3-甲氧基苯基)乙醇合成路线 （共 28 条）
反应条件
phosphate buffer; Daucus carota L in acetone pH=6.5; 48 h; Enzymatic reaction;
参考文献
Maczka, Wanda K.; Mironowicz, Agnieszka
Tetrahedron Asymmetry, 2004 , vol. 15, # 13 p. 1965 - 1967
反应条件
benzo[1,3,2]dioxaborole; chiral catalyst 1a in hexane T=-30°C; 1 h; different titanium alkoxide catalysts, other solvents and reaction time; also reduction of further ketones; Product distribution;
参考文献
Angewandte Chemie, , vol. 107, # 18 p. 2165 - 2166
反应条件
bis(acetylacetonate)nickel(II); C64H93NO8P2 in tetrahydrofuran T=-20°C; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Tetrahedron Letters, , vol. 50, # 31 p. 4495 - 4497
反应条件
1: With bis(acetylacetonate)nickel(II); C30H44NO7PSi2 in tetrahydrofuran T=5°C; Inert atmosphere; 2: With hydrogenchloride in tetrahydrofuran; water optical yield given as percent eeenantioselective reaction;
参考文献
Tetrahedron Asymmetry, , vol. 20, # 13 p. 1575 - 1579
反应条件
titanium(IV) isopropylate; 1-((S)-2-((R)-hydroxy(naphthalen-2-yl)methyl)naphthalen-1-yl)naphthalen-2-ol in toluene T=-40°C; Schlenk technique; enantioselective reaction;
参考文献
Zheng, Long-Sheng; Jiang, Ke-Zhi; Deng, Yuan; Bai, Xing-Feng; Gao, Guang; Gu, Feng-Lei; Xu, Li-Wen
European Journal of Organic Chemistry, 2013 , # 4 p. 748 - 750
反应条件
Arthrobacter atrocyaneus in aq. phosphate buffer T=32°C; 72 h; Microbiological reaction; enantioselective reaction;
参考文献
Silva, Camila R.; Souza, Juliana C.; Araujo, Lidiane S.; Kagohara, Edna; Garcia, Thais P.; Pelizzari, Vivian H.; Andrade, Leandro H.
Journal of Molecular Catalysis B: Enzymatic, 2012 , vol. 83, p. 23 - 28
反应条件
bis(norbornadiene)rhodium(I) tetrafluoroborate; C67H63N2O7P; C71H71N2O7P; diethylzinc; 4,4,5,5-tetramethyl-[1,3,2]dioxaborolane in tetrahydrofuran T=0 - 20°C; Inert atmosphere; optical yield given as percent ee;
参考文献
Moteki, Shin A.; Toyama, Kazuya; Liu, Zeyu; Ma, Jing; Holmes, Andrea E.; Takacs, James M.
Chemical Communications, 2012 , vol. 48, # 2 p. 263 - 265
反应条件
trans-(R, R)-[Fe(Ph2PCH2CH=NCH(Ph)CH(Ph)N=CHCH2PPh2)(CH3CN)(CO)][BPh4]2; potassium tert-butylate in isopropyl alcohol T=22°C; 0.5 h; Inert atmosphere; optical yield given as percent ee;
参考文献
Journal of the American Chemical Society, , vol. 131, # 4 p. 1394 - 1395
反应条件
1: dimethyl zinc With (2S)-1-(ferrocenylmethyl)aziridin-2-yl(diphenyl)methanol in toluene T=0 - 40°C; Inert atmosphere; 2: 3-methoxy-benzaldehyde in toluene T=0 - 30°C; 3: With water; ammonium chloride in toluene optical yield given as percent eeenantioselective reaction;
参考文献
Wang, Min-Can; Zhang, Qing-Jian; Li, Gao-Wei; Liu, Zhi-Kang
Tetrahedron Asymmetry, 2009 , vol. 20, # 3 p. 288 - 292
反应条件
titanium(IV) isopropylate; (S)-(+)-N-benzylmandelamide in dichloromethane; toluene T=0°C; 24 h; Title compound not separated from byproducts;
参考文献
Tetrahedron Asymmetry, , vol. 16, # 11 p. 1953 - 1958
