反应条件
1: 1.) mercuric acetate, water, 2.) sodium borohydride / 1.) water, THF, 7 min, 2.) 2 h
2: 63 percent / lithium, ammonia / tetrahydrofuran / 3 h / -33 °C
3: 1.4 g / pyridine / 15 h / Ambient temperature
4: 1.) thionyl chloride, pyridine, 2.) LAH / 1.) ether 0 deg C, 10 min
5: pyridine
6: LiAlH4
7: pyridine
8: 63 percent / lithium, liq. ammonia / tetrahydrofuran; ethanol / 0.5 h
View Scheme
参考文献
Dimitriadis; Massy-Westropp
Australian Journal of Chemistry, 1980 , vol. 33, # 12 p. 2729 - 2736
