2,3,5,6-四氟茴香醚合成路线 (共 25 条)
反应条件
in methanol; dimethylsulfoxide-d6 Kinetics;
参考文献
Tetrahedron Letters, , vol. 47, # 42 p. 7405 - 7407
反应条件
in methanol; dimethylsulfoxide-d6 Kinetics;
参考文献
Tetrahedron Letters, , vol. 47, # 42 p. 7405 - 7407
反应条件
in methanol; dimethylsulfoxide-d6 Kinetics;
参考文献
Tetrahedron Letters, , vol. 47, # 42 p. 7405 - 7407
反应条件
in methanol; dimethylsulfoxide-d6 Kinetics;
参考文献
Tetrahedron Letters, , vol. 47, # 42 p. 7405 - 7407
反应条件
boron trifluoride; nitric acid; nitrogen(IV) oxide in sulfolane
参考文献
Coe,P.L.; Jukes,A.E.
Tetrahedron, 1968 , vol. 24, p. 5913 - 5916
反应条件
(i) (CF3SO3)3Tl, (ii) aq. NaI; Multistep reaction;
参考文献
Deacon,G.B.; Tunaley,D.
Australian Journal of Chemistry, 1979 , vol. 32, p. 737 - 753
反应条件
1,10-phenanthroline; oxygen; 2,3-dicyano-5,6-dichloro-p-benzoquinone; copper dichloride; lithium tert-butylate in dimethyl sulfoxide T=40°C; P=760.051 Torr; 12 h;
参考文献
Journal of the American Chemical Society, , vol. 132, p. 2522 - 2523
反应条件
iodine; lithium tert-butylate in N,N-dimethyl-formamide T=60°C; 1 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 11, # 2 p. 421 - 423
反应条件
C12H22N(1-)*Cl(1-)*Mg(2+)*ClLi; oxygen; copper dichloride; zinc(II) chloride T=20°C; Glaser-Hay Coupling; P=760.051 Torr; Inert atmosphere;
参考文献
Do, Hien-Quang; Daugulis, Olafs
Journal of the American Chemical Society, 2009 , vol. 131, # 47 p. 17052 - 17053
反应条件
1: 1,2,4,5-tetrafluoro-3-methoxybenzene With oxygen; copper dichloride; lithium tert-butylate in N,N-dimethyl-formamide T=20°C; Inert atmosphere; 2: trifluoroacetic acid in ethyl acetate
参考文献
Journal of the American Chemical Society, , vol. 131, # 47 p. 17052 - 17053