4,5,7-邻乙酰基-2,6-酐-3-脱氧-d-lyxo-2-庚烯腈合成路线 (共 6 条)
反应条件
hydrogen bromide in acetic acid 0.25 h; Ambient temperature;
参考文献
Viladot, Josep-Lluis; Moreau, Vincent; Planas, Antoni; Driguez, Hugues
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 16 p. 2383 - 2387
反应条件
hydrogen bromide in acetic acid T=0°C; 2 h;
参考文献
Rychener, Martin; Bigler, Peter; Pfander, Hanspeter
Helvetica Chimica Acta, 1984 , vol. 67, # 2 p. 378 - 385
反应条件
hydrogen bromide in acetic acid; 1,2-dichloro-ethane 3 h; Ambient temperature;
参考文献
Wang; Sakairi; Kuzuhara
Carbohydrate Research, 1991 , vol. 219, p. 133 - 148
反应条件
pyridine; hydrogen bromide; acetic acid 2.) 1.5 h, 15-20 deg C; Yield given. Multistep reaction;
参考文献
Ogawa, Tomoya; Kaburagi, Toshiaki
Carbohydrate Research, 1982 , vol. 103, p. 53 - 64
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in dichloromethane 4 h; Heating;
参考文献
Viladot, Josep-Lluis; Moreau, Vincent; Planas, Antoni; Driguez, Hugues
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 16 p. 2383 - 2387
反应条件
1: 45 percent / benzyltriethylammonium chloride, aq. NaOH / CH2Cl2 / 4 h / Heating 2: 62 percent / NaOMe / methanol / 7 h / Ambient temperature View Scheme
参考文献
Viladot, Josep-Lluis; Moreau, Vincent; Planas, Antoni; Driguez, Hugues
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 16 p. 2383 - 2387