(E)-9-十四碳烯-1-醇乙酸酯合成路线 （共 31 条）
反应条件
1: 51 percent / hexane / 4 h / Heating
2: 83 percent / bromine, triphenylphosphine / CH2Cl2 / 0 °C / 1.) 0 deg C, 1 h 2.) room temp., 1 h
4: 85 percent / pyridine / 3 h / Ambient temperature
View Scheme
参考文献
Chattopadhyay, A.; Mamdapur, V. R.; Chadha, M. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 12 p. 1221 - 1223
反应条件
1: 83 percent / bromine, triphenylphosphine / CH2Cl2 / 0 °C / 1.) 0 deg C, 1 h 2.) room temp., 1 h
3: 85 percent / pyridine / 3 h / Ambient temperature
View Scheme
参考文献
Chattopadhyay, A.; Mamdapur, V. R.; Chadha, M. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 12 p. 1221 - 1223
反应条件
1: 79 percent / conc. HCl / 3 h / Ambient temperature
3: 85 percent / pyridine / 3 h / Ambient temperature
View Scheme
参考文献
Chattopadhyay, A.; Mamdapur, V. R.; Chadha, M. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 12 p. 1221 - 1223
反应条件
Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Chan, Tak-Hang; Huang, Wen-Qiang
Journal of the Chemical Society, Chemical Communications, 1985 , # 13 p. 909 - 911
反应条件
2: 85 percent / pyridine / 3 h / Ambient temperature
View Scheme
参考文献
Chattopadhyay, A.; Mamdapur, V. R.; Chadha, M. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 12 p. 1221 - 1223
反应条件
2: 85 percent / pyridine / 3 h / Ambient temperature
View Scheme
参考文献
Chattopadhyay, A.; Mamdapur, V. R.; Chadha, M. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 12 p. 1221 - 1223
反应条件
Yield given. Multistep reaction;
参考文献
Sonnet, Philip E.
Journal of Organic Chemistry, 1980 , vol. 45, # 1 p. 154 - 157
反应条件
sodium methylate
1) DMF, 25 deg C, 2 h; 2) DMF, 0 deg C, 4 h.; Yield given. Multistep reaction;
参考文献
Dzhumakulov, T.; Yuldashev, A. M.; Abduvakhabov, A. A.
Chemistry of Natural Compounds, 1982 , vol. 18, # 4 p. 516 - 517
Khimiya Prirodnykh Soedinenii, 1982 , vol. 18, # 4 p. 538 - 539
反应条件
Cl2Ni(1,2-bis(diphenylphosphino)ethane)
1.) ether, 12 h, room temp., 2.) 80 deg C, 15 h; Yield given. Multistep reaction;
参考文献
Fiandanese, Vito; Marchese, Giuseppe; Naso, Francesco; Ronzini, Ludovico
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1115 - 1120
反应条件
Cl2Ni(1,2-bis(diphenylphosphino)ethane)
1.) ether, 12 h, room temp., 2.) 80 deg C, 15 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Fiandanese, Vito; Marchese, Giuseppe; Naso, Francesco; Ronzini, Ludovico
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1115 - 1120
