(E)-9-十四碳烯-1-醇乙酸酯合成路线 （共 31 条）
反应条件
pyridinium chlorochromate in hexane; dichloromethane
参考文献
Phillips Petroleum Company
Patent: US4560792 A1, 1985 ;
反应条件
pyridine in diethyl ether
参考文献
Rossi, Renzo; Carpita, Adriano; Gaudenzi, Loretta; Quirici, Maria Grazia
Gazzetta Chimica Italiana, 1980 , vol. 110, # 4 p. 237 - 246
参考文献
Singh, Krishna Nand; Singh, Manorama; Misra, Ram Achal
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1993 , vol. 32, # 4 p. 431 - 434
反应条件
1: 76 percent / PdCl2(PPh3)2 / diethyl ether; tetrahydrofuran / 1 h / Ambient temperature
2: 1.) NiCl2(Ph2PCH2CH2PPh2) / 1.) ether, 12 h, room temp., 2.) 80 deg C, 15 h
View Scheme
参考文献
Fiandanese, Vito; Marchese, Giuseppe; Naso, Francesco; Ronzini, Ludovico
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1115 - 1120
反应条件
WCl4(O-2,6-C6H3Cl2)2; tetramethylstannane in chlorobenzene
T=85°C; 5 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Crisp, Geoffrey T.; Collis, Maree P.
Australian Journal of Chemistry, 1988 , vol. 41, # 6 p. 935 - 942
反应条件
1: 84.9 percent / LiAlH4 / diethyl ether
2: 86.6 percent / pyridine / benzene
View Scheme
参考文献
Singh, Krishna Nand; Singh, Manorama; Misra, Ram Achal
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1993 , vol. 32, # 4 p. 431 - 434
参考文献
Chan, Tak-Hang; Huang, Wen-Qiang
Journal of the Chemical Society, Chemical Communications, 1985 , # 13 p. 909 - 911
反应条件
1: 63 percent / DMSO, NaH / tetrahydrofuran / 0.5 h
2: pyridine
View Scheme
参考文献
Horiike; Tanouchi; Hirano
Agricultural and Biological Chemistry, 1980 , vol. 44, # 2 p. 257 - 261
反应条件
1: 90 percent / acetonitrile
2: 63 percent / DMSO, NaH / tetrahydrofuran / 0.5 h
3: pyridine
View Scheme
参考文献
Horiike; Tanouchi; Hirano
Agricultural and Biological Chemistry, 1980 , vol. 44, # 2 p. 257 - 261
反应条件
1: 63 percent / DMSO, NaH / tetrahydrofuran / 0.5 h
2: pyridine
View Scheme
参考文献
Horiike; Tanouchi; Hirano
Agricultural and Biological Chemistry, 1980 , vol. 44, # 2 p. 257 - 261
