2,6-二溴-4-(羟基甲基)苯酚合成路线 (共 10 条)
反应条件
sodium tetrahydroborate in ethanol T=20°C; Inert atmosphere;
参考文献
Akai, Shuji; Ikawa, Takashi; Takayanagi, Sho-Ichi; Morikawa, Yuki; Mohri, Shinya; Tsubakiyama, Masaya; Egi, Masahiro; Wada, Yasufumi; Kita, Yasuyuki
Angewandte Chemie - International Edition, 2008 , vol. 47, # 40 p. 7673 - 7676
反应条件
1: Br2, aq. HBr / ethanol 2: NaBH4 / ethanol View Scheme
参考文献
Higa,T.; Scheuer,P.J.
Tetrahedron, 1975 , vol. 31, p. 2379 - 2381
反应条件
1: 81 percent / DDQ / methanol / 1 h / Ambient temperature 2: 88 percent / NaBH4 / methanol View Scheme
参考文献
Sudalai, A.; Rao, G. S. Krishna
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, # 1-11 p. 858 - 859
参考文献
Auwers; Daecke
Chemische Berichte, 1899 , vol. 32, p. 3377
参考文献
Auwers; Daecke
Chemische Berichte, 1899 , vol. 32, p. 3377
反应条件
sodium hydroxide; nickel monoaluminide
参考文献
Finn; Musty
Journal of Applied Chemistry, 1952 , vol. 2, p. 88
参考文献
Autenrieth; Beuttel
Archiv der Pharmazie (Weinheim, Germany), 1910 , vol. 248, p. 123
反应条件
2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; copper diacetate in water; acetonitrile T=20°C; 4 h; Green chemistry;
参考文献
Jiang, Jian-An; Du, Jia-Lei; Wang, Zhan-Guo; Zhang, Zhong-Nan; Xu, Xi; Zheng, Gan-Lin; Ji, Ya-Fei
Tetrahedron Letters, 2014 , vol. 55, # 10 p. 1677 - 1681
反应条件
2: nickel-aluminium-alloy; aqueous NaOH View Scheme
参考文献
Zigeuner et al.
Monatshefte fuer Chemie, 1959 , vol. 90, p. 473,478
反应条件
Fremy’s salt in chloroform
3 h;
参考文献
Saa, Jose M.; Morey, Jeronimo; Costa, Antonio
Tetrahedron Letters, 1986 , vol. 27, # 42 p. 5125 - 5128