2-(3-甲基苯基)-1H-异吲哚-1,3(2H)-二酮合成路线 （共 9 条）
反应条件
1: With water; potassium carbonate in acetone 0.166667 h; Sonication; 2: in acetone T=15 - 20°C; 2 h; UV-irradiationInert atmosphere;
参考文献
Lee, Yong-Jun; Ahn, Do-Hwan; Lee, Kyoung-Sub; Kim, Ae Rhan; Yoo, Dong Jin; Oelgemoeller, Michael
Tetrahedron Letters, 2011 , vol. 52, # 39 p. 5029 - 5031
反应条件
pyridine; oxygen; copper diacetate in dichloromethane 168 h;
参考文献
Huegel, Helmut M.; Rix, Colin J.; Fleck, Karin
Synlett, 2006 , # 14 p. 2290 - 2292
参考文献
Tingle; Rolker
Journal of the American Chemical Society, 1908 , vol. 30, p. 1889
反应条件
air in benzene T=20°C; 48 h;
参考文献
Doepp, Dietrich; Hassan, Alaa A.; Mourad, Aboul-Fetouh E.; Nour El-Din, Ahmed M.; Angermund, Klaus; Krueger, Carl; Lehmann, Christian W.; Rust, Joerg
Tetrahedron, 2003 , vol. 59, # 27 p. 5073 - 5081
反应条件
acetic acid Heating;
参考文献
Capitosti, Scott M.; Hansen, Todd P.; Brown, Milton L.
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 2 p. 327 - 336
反应条件
[iridium(III)(2-phenylpyridine)3] in acetonitrile T=20°C; 24 h; Sealed tubeIrradiation; Overall yield = 80percent; regioselective reaction;
参考文献
Allen, Laura J.; Cabrera, Pablo J.; Lee, Melissa; Sanford, Melanie S.
Journal of the American Chemical Society, 2014 , vol. 136, # 15 p. 5607 - 5610
反应条件
[bis(acetoxy)iodo]benzene T=140°C; 4 h; chemoselective reaction;
参考文献
Shrestha, Ruja; Mukherjee, Paramita; Tan, Yichen; Litman, Zachary C.; Hartwig, John F.
Journal of the American Chemical Society, 2013 , vol. 135, # 23 p. 8480 - 8483
反应条件
1: acetonitrile / 4 h / 20 °C / |Schlenk technique; |Inert atmosphere 2: [iridium(III)(2-phenylpyridine)3] / acetonitrile / 24 h / 20 °C / |Sealed tube; |Irradiation View Scheme
参考文献
Allen, Laura J.; Cabrera, Pablo J.; Lee, Melissa; Sanford, Melanie S.
Journal of the American Chemical Society, 2014 , vol. 136, # 15 p. 5607 - 5610
参考文献
Tingle; Rolker
Journal of the American Chemical Society, 1908 , vol. 30, p. 1889
