2-丁基硫基-1,3-苯并噻唑合成路线 (共 11 条)
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; Na2S2O3 pentahydrate; caesium carbonate in ethylene glycol; dimethyl sulfoxide T=120°C; Schlenk techniqueInert atmosphereGreen chemistry;
参考文献
Qiao, Zongjun; Wei, Jianpeng; Jiang, Xuefeng
Organic Letters, 2014 , vol. 16, # 4 p. 1212 - 1215
反应条件
N-ethyl-N,N-diisopropylamine in acetone T=20°C; 0.25 h; Sonication;
参考文献
Deligeorgiev, Todor; Kaloyanova, Stefka; Lesev, Nedyalko; Vaquero, Juan J.
Ultrasonics Sonochemistry, 2010 , vol. 17, # 5 p. 783 - 788
反应条件
[2,2']bipyridinyl; copper(l) iodide; oxygen; sodium carbonate in N,N-dimethyl-formamide T=140°C; 24 h;
参考文献
Ranjit, Sadananda; Lee, Richmond; Heryadi, Dodi; Shen, Chao; Wu, Ji'En; Zhang, Pengfei; Huang, Kuo-Wei; Liu, Xiaogang
Journal of Organic Chemistry, 2011 , vol. 76, # 21 p. 8999 - 9007
反应条件
N-benzyl-trimethylammonium hydroxide T=20°C; Neat (no solvent);
参考文献
Meshram; Reddy, B. Chennakesava; Goud, P. Ramesh
Synthetic Communications, 2009 , vol. 39, # 13 p. 2297 - 2303
反应条件
CuO; potassium carbonate in N,N-dimethyl-formamide T=140°C; 48 h; Inert atmosphereSchlenk technique;
参考文献
Rosario, Alisson R.; Casola, Kamila K.; Oliveira, Carla E.S.; Zeni, Gilson
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 14-15 p. 2960 - 2966
反应条件
sodium hydroxide; Amberlite IRA-400 chloride form in water; acetone
参考文献
Dalal; Pawar; Mahulikar
Organic Preparations and Procedures International, 2005 , vol. 37, # 6 p. 539 - 546
反应条件
potassium carbonate; 1-n-butyl-3-methylimidazolium hexafluorophosphate T=50°C; 7 h;
参考文献
Hu, Yi; Chen, Zhen-Chu; Le, Zhang-Gao; Zheng, Qin-Guo
Synthetic Communications, 2004 , vol. 34, # 11 p. 2039 - 2046
反应条件
copper diacetate; silver trifluoroacetate in N,N-dimethyl-formamide T=120°C; 12 h; Inert atmosphere;
参考文献
Dai, Chao; Xu, Zhaoqing; Huang, Fei; Yu, Zhengkun; Gao, Yan-Feng
Journal of Organic Chemistry, 2012 , vol. 77, # 9 p. 4414 - 4419
参考文献
Torii, Sigeru; Sayo, Noboru; Tanaka, Hideo
Chemistry Letters, 1980 , p. 695 - 698
参考文献
Ettel et al.
Chemicke Listy, 1952 , vol. 46, p. 756
Chem.Abstr., 1953 , p. 12358