2-乙酰基-5-硝基苯并[b]呋喃合成路线 （共 9 条）
反应条件
potassium hydroxide in methanol 48 h; Heating;
参考文献
Paizs, Csaba; Tosa, Monica; Majdik, Cornelia; Moldovan, Paula; Novak, Lajos; Kolonits, Pal; Marcovici, Adriana; Irimie, Florin-Dan; Poppe, Laszlo
Tetrahedron Asymmetry, 2003 , vol. 14, # 11 p. 1495 - 1501
反应条件
1: 2-hydroxy-5-nitro-benzaldehyde With potassium hydroxide in ethanol Aldol Condensation; 0.25 h; Cooling with ice; 2: 1-bromo-2-propanone With potassium iodide in ethanol Aldol Condensation; Cooling;
参考文献
Aruna Kumar; Desai, Nivedita R.; Krishnaswamy; Sreenivasa; Mahadevan
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2014 , vol. 53, # 4 p. 426 - 430
反应条件
nitric acid in acetic anhydride 3 h; Ambient temperature;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 33, # 7 p. 2854 - 2861
反应条件
potassium fluoride in methanol T=20°C; 192 h;
参考文献
Lamotte, Genevieve; Demerseman, Pierre; Royer, Rene
Synthesis, 1984 , # 12 p. 1068 - 1070
反应条件
nitric acid; tin(IV) chloride in dichloromethane T=0°C; 2 h;
参考文献
Canadian Journal of Chemistry, , vol. 61, p. 2287 - 2290
反应条件
nitric acid; tin(IV) chloride in dichloromethane T=0°C; 4 h;
参考文献
Canadian Journal of Chemistry, , vol. 61, p. 2287 - 2290
反应条件
in xylene 0.5 h; Heating;
参考文献
Capuano, Lilly; Ahlhelm, Alfred; Hartmann, Herbert
Chemische Berichte, 1986 , vol. 119, # 6 p. 2069 - 2074
反应条件
1: 86 percent / 115 °C 2: 68 percent / xylene / 0.5 h / Heating View Scheme
参考文献
Chemische Berichte, , vol. 119, # 6 p. 2069 - 2074
反应条件
1: 1.) 80 percent hydrazine hydrate; 2.) KOH / 1.) 125 deg C, 1.5 h; 2.) 140 deg C, 1 h
2: 52.7 percent / AlCl3 / CS2 / 24 h / 25 °C
View Scheme
参考文献
Ohishi; Kuriyama; Doi; Nakanishi
Chemical and Pharmaceutical Bulletin, 1985 , vol. 33, # 7 p. 2854 - 2861
