2-羟基-4,6-二甲氧基-3-甲基苯乙酮合成路线 (共 26 条)
反应条件
aluminium trichloride; benzene
参考文献
Mukerjee et al.
Proceedings - Indian Academy of Sciences, Section A, 1953 , vol. 37, p. 127,141
反应条件
aluminium trichloride in diethyl ether
10 h; Ambient temperature;
参考文献
Kawamura; Takatsuki; Torii; Horie
Bulletin of the Chemical Society of Japan, 1994 , vol. 67, # 2 p. 511 - 515
反应条件
boron trifluoride; acetic acid
参考文献
Dean; Robertson
Journal of the Chemical Society, 1953 , p. 1241,1245
反应条件
1: AlBr3 / acetonitrile / 5 h / 20 °C
2: (C2H5)3SiH / trifluoroacetic acid / 20 °C
3: BF3*Et2O
View Scheme
参考文献
Mateeva, Nelly N.; Kode, Rao N.; Redda, Kinfe K.
Journal of Heterocyclic Chemistry, 2002 , vol. 39, # 6 p. 1251 - 1258
反应条件
sodium hydroxide; tetra-(n-butyl)ammonium iodide in dichloromethane; water
T=20°C; 24 h;
参考文献
Vogel, Susanne; Heilmann, Joerg
Journal of Natural Products, 2008 , vol. 71, # 7 p. 1237 - 1241
反应条件
in methanol; diethyl ether; ethyl acetate
T=0 - 20°C;
参考文献
Nakagawa-Goto, Kyoko; Lee, Kuo-Hsiung
Tetrahedron Letters, 2006 , vol. 47, # 47 p. 8263 - 8266
反应条件
1: (C2H5)3SiH / trifluoroacetic acid / 20 °C
2: BF3*Et2O
View Scheme
参考文献
Mateeva, Nelly N.; Kode, Rao N.; Redda, Kinfe K.
Journal of Heterocyclic Chemistry, 2002 , vol. 39, # 6 p. 1251 - 1258
反应条件
potassium carbonate in acetone
3 h; Heating; Yield given. Yields of byproduct given;
参考文献
Tada, Akihiro; Saitoh, Tamotsu; Shoji, Junzo
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 8 p. 2487 - 2493
反应条件
potassium carbonate in acetone
3 h; Heating;
参考文献
Hossain, M. Amzad
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2001 , vol. 40, # 4 p. 324 - 326
反应条件
potassium carbonate; acetone
参考文献
Curd; Robertson
Journal of the Chemical Society, 1933 , p. 437,440
Full Text Show Details
Gruber; Traub
Monatshefte fuer Chemie, 1947 , vol. 77, p. 414,423