甲基N-甲酰基苯丙氨酸酯合成路线 (共 15 条)
反应条件
hydroxylamine hydrochloride; sodium acetate in methanol
参考文献
Ajinomoto Co., Inc.
Patent: US4021418 A1, 1977 ;
反应条件
hydrogenchloride in methanol 1 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 71, # 5 p. 2026 - 2036
反应条件
γ-Fe2O3@HAp-SO3H in water
T=20°C; 0.666667 h;
参考文献
Pathare, Sagar P.; Sawant, Ravindra V.; Akamanchi, Krishnacharya G.
Tetrahedron Letters, 2012 , vol. 53, # 26 p. 3259 - 3263
反应条件
4-methyl-morpholine; 4-(N,N-dimethlyamino)pyridine; 2-chloro-4,6-dimethoxy-[1,3,5]triazine; triethylamine in dichloromethane
T=35°C; 0.1 h; microwave irradiation;
参考文献
De Luca, Lidia; Giacomelli, Giampaolo; Porcheddu, Andrea; Salaris, Margherita
Synlett, 2004 , # 14 p. 2570 - 2572
反应条件
in toluene
4.5 h; Heating / reflux;
参考文献
LA JOLLA PHARMACEUTICAL COMPANY
Patent: WO2005/82343 A2, 2005 ;
Location in patent: Page/Page column 96 ;
反应条件
triethylamine in chloroform
T=0 - 10°C; 3 h;
参考文献
Karim, A.; Mortreux, A.; Petit, F.; Buono, G.; Pfeiffer, G.; Siv, C.
Journal of Organometallic Chemistry, 1986 , vol. 317, p. 93 - 104
反应条件
anhydrous magnesium perchlorate in N,N-dimethyl-formamide
Ambient temperature;
参考文献
Giesemann, Gerhard; Ugi, Ivar
Synthesis, 1983 , # 10 p. 788 - 789
反应条件
triethylamine in dichloromethane
12 h; Ambient temperature;
参考文献
Duczek; Deutsch; Vieth; Niclas
Synthesis, 1996 , # 1 p. 37 - 38
参考文献
Zeeberg; Caplow; Caswell
Journal of the American Chemical Society, 1975 , vol. 97, # 25 p. 7346 - 7352
反应条件
triethylamine in water; acetonitrile
T=40°C;
参考文献
Kotlova, E. K.; Levin, E. D.; Yusupova, M. P.; Rozynov, B. V.; Stepanov, V. M.
Russian Journal of Bioorganic Chemistry, 1994 , vol. 20, # 11 p. 678 - 686
Bioorganicheskaya Khimiya, 1994 , vol. 20, # 11 p. 1186 - 1195