3,6-二(苯基甲基)哌嗪-2,5-二酮合成路线 （共 11 条）
反应条件
bei trockner Destillation; active (?) form from l-phenylalanine;
参考文献
Cao, Yanchun; Cao, Shuxia; Xie, Yali; Zong, Xiangkun; Zhao, Yufen
Chinese Journal of Chemistry, 2011 , vol. 29, # 6 p. 1173 - 1179
反应条件
1,2-diamino-benzene T=180°C; 1 h;
参考文献
Nawwar, Galal A. M.; Shalabi, Ahmed M.; Ahmed, Sayed A. H.
Journal of Chemical Research, Miniprint, 1993 , # 7 p. 1533 - 1551
反应条件
1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 6 h / 20 °C / Cooling with ice 2: piperidine / dichloromethane / 2 h View Scheme
参考文献
JAWAHARLAL NEHRU CENTRE FOR ADVANCED SCIENTIFIC RESEARCH; GOVINDARAJU, Thimmaiah
Patent: WO2011/55247 A1, 2011 ;
反应条件
bei trockner Destillation; inactive form;
参考文献
Ohta, Akihiro; Kojima, Akihiko; Aoyagi, Yutaka
Heterocycles, 1990 , vol. 31, # 9 p. 1655 - 1662
参考文献
Sasaki
Chemische Berichte, 1921 , vol. 54, p. 164
反应条件
T=180°C; inactive form;
参考文献
Fischer,E.
Chemische Berichte, 1901 , vol. 34, p. 450
反应条件
1: acetic acid anhydride; sodium acetate / 120 - 130 °C 2: zinc dust; glacial acetic acid View Scheme
参考文献
Sasaki
Chemische Berichte, 1921 , vol. 54, p. 164
反应条件
bei trockner Destillation;
参考文献
Erlenmeyer senior; Lipp
Justus Liebigs Annalen der Chemie, 1883 , vol. 219, p. 188,194
反应条件
Hydrogenation; 3.6-dioxo-2.5-dibenzylidene-piperazine;
参考文献
Sasaki
Chemische Berichte, 1921 , vol. 54, p. 164
反应条件
bei der trocknen Destillation;
参考文献
Schulze; Barbieri
Chemische Berichte, 1881 , vol. 14, p. 1789
Journal fuer Praktische Chemie (Leipzig), 1883 , vol. <2> 27, p. 345
Full Text Show Details
Schulze; Barbieri
Chemische Berichte, 1883 , vol. 16, p. 1714
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, 1885 , vol. 9, p. 101
Full Text Show Details
Schulze
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, 1885 , vol. 9, p. 66,98
