N-甲基-4-氨基邻苯二甲酰亚胺合成路线 (共 13 条)
反应条件
hydrogenchloride; water; tin(ll) chloride T=20°C;
参考文献
Duan, Xin-Hong; Qiao, Jin-Ping; Yang, Yang; Cui, Meng-Chao; Zhou, Jiang-Ning; Liu, Bo-Li
Bioorganic and Medicinal Chemistry, 2010 , vol. 18, # 3 p. 1337 - 1343
参考文献
University of Kentucky Research Foundation
Patent: US7759468 B1, 2010 ;
反应条件
ammonium hydroxide T=280 - 290°C;
参考文献
Journal of the American Chemical Society, , vol. 30, p. 1143
反应条件
1: 60 percent / K2CO3 / dimethylformamide / 1 h / 130 °C 2: 1.) SnCl2, HCl, 2.) H2O View Scheme
参考文献
Chemische Berichte, , vol. 117, # 6 p. 2275 - 2286
反应条件
1.1: nitric acid; sulfuric acid / 16 h / 5 - 20 °C 2.1: potassium hydroxide / methanol; ethanol / 3 h / 20 °C 2.2: 1 h / |Reflux 3.1: palladium on activated charcoal; ammonium formate / tetrahydrofuran / 12 h / 20 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 23, # 7 p. 2022 - 2026
参考文献
Journal of the American Chemical Society, , vol. 30, p. 1143
反应条件
sulfuric acid T=150°C; 0.0416667 h; Title compound not separated from byproducts;
参考文献
Russian Journal of General Chemistry, , vol. 65, # 3.2 p. 454 - 456
Zhurnal Obshchei Khimii, , vol. 65, # 3 p. 511 - 513
反应条件
sulfuric acid T=150°C; 0.0416667 h; Title compound not separated from byproducts;
参考文献
El'tsov, A. V.; Martynova, V. P.; Sokolova, N. B.; Dmitrieva, N. M.; Brykov, A. S
Russian Journal of General Chemistry, 1995 , vol. 65, # 3.2 p. 454 - 456
Zhurnal Obshchei Khimii, 1995 , vol. 65, # 3 p. 511 - 513
参考文献
Bogert; Renshaw
Journal of the American Chemical Society, 1908 , vol. 30, p. 1143
反应条件
copper(I) bromide Diazotization;
参考文献
Tirouflet; Dabard
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1956 , vol. 242, p. 916