5,5-二甲氧基戊酸甲酯合成路线 （共 19 条）
参考文献
Tetrahedron Letters, , vol. 28, # 16 p. 1821 - 1824
反应条件
(i) Pb(OAc)4, MeOH, (ii) /BRN= 1098229/, H2SO4; Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 35, p. 973 - 978
反应条件
hydrogenchloride; ozone -78 deg to r.t.; Product distributionMechanism;
参考文献
Chemische Berichte, , vol. 115, # 8 p. 2697 - 2706
反应条件
aniline in hexadeuterioacetone; dichloromethane; carbon dioxide; water liquid CO2;
参考文献
US2014/142147 A1, ;
Page/Page column ;
反应条件
1: CF3SO3H, H2O / tetrahydrofuran / 5 h / 17 - 22 °C
2: t-BuNH2BH3 / tetrahydrofuran; H2O / 10 - 15 °C
View Scheme
参考文献
Lukin, Kirill A.; Yang, ChengXi; Bellettini, John R.; Narayanan; Leanna, M. Robert; Rasmussen, Michael
Synlett, 1999 , # 1 p. 59 - 60
反应条件
sodium hydroxide in methanol
2 h; Ambient temperature;
参考文献
Cabezas, Edelmira; Satterthwait, Arnold C.
Journal of the American Chemical Society, 1999 , vol. 121, # 16 p. 3862 - 3875
反应条件
1: 94 percent / LiAlH4 / diethyl ether / 1) -78 deg C to 0 deg C, 0 deg C, 6 h, 2) r.t., 12 h
2: 86 percent / pyridine / 2 h / -20 °C
3: 96 percent / LiBr / acetone / 2.5 h / Ambient temperature
View Scheme
参考文献
Beifuss, Uwe; Gehm, Henning; Herde, Andreas; Ledderhose, Sabine
Journal fur Praktische Chemie - Chemiker - Zeitung, 1996 , vol. 338, # 5 p. 468 - 478
反应条件
2,4-dinitrobenzenesulfonic acid in acetonitrile
T=20°C; Hosomi-Sakurai reaction; 3 h;
参考文献
Kampen, Daniela; List, Benjamin
Synlett, 2006 , # 16 p. 2589 - 2592
反应条件
trifluorormethanesulfonic acid; water in tetrahydrofuran
T=17 - 22°C; 5 h;
参考文献
Lukin, Kirill A.; Yang, ChengXi; Bellettini, John R.; Narayanan; Leanna, M. Robert; Rasmussen, Michael
Synlett, 1999 , # 1 p. 59 - 60
